(4R,5R)-5-Benzyloxy-4-((R)-1-methoxymethoxy-pentadecyl)-2,2-dimethyl-[1,3]dioxane

Base Information

Chemical Name:(4R,5R)-5-Benzyloxy-4-((R)-1-methoxymethoxy-pentadecyl)-2,2-dimethyl-[1,3]dioxane
CAS No.:169238-11-3
Molecular Formula:C₃₀H₅₂O₅
Molecular Weight:492.74
Hs Code.:

Synonyms:(4R,5R)-5-Benzyloxy-4-((R)-1-methoxymethoxy-pentadecyl)-2,2-dimethyl-[1,3]dioxane

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Chemical Property of (4R,5R)-5-Benzyloxy-4-((R)-1-methoxymethoxy-pentadecyl)-2,2-dimethyl-[1,3]dioxane

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Technology Process of (4R,5R)-5-Benzyloxy-4-((R)-1-methoxymethoxy-pentadecyl)-2,2-dimethyl-[1,3]dioxane

There total 7 articles about (4R,5R)-5-Benzyloxy-4-((R)-1-methoxymethoxy-pentadecyl)-2,2-dimethyl-[1,3]dioxane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 107-30-2
chloromethyl methyl ether

: 161459-71-8
(R)-1-((4R,5R)-5-Benzyloxy-2,2-dimethyl-[1,3]dioxan-4-yl)-pentadecan-1-ol

: 169238-11-3
(4R,5R)-5-Benzyloxy-4-((R)-1-methoxymethoxy-pentadecyl)-2,2-dimethyl-[1,3]dioxane

Guidance literature:: With N-ethyl-N,N-diisopropylamine;
DOI:10.1016/0040-4039(94)88514-1

Reference yield:

: 2-(benzyloxy)-1-(trimethylsiloxy)-1-phenoxyethylene

: 169238-11-3
(4R,5R)-5-Benzyloxy-4-((R)-1-methoxymethoxy-pentadecyl)-2,2-dimethyl-[1,3]dioxane

Guidance literature:: Multi-step reaction with 6 steps

1: 80 percent / Sn(OTf)2, SnO, chiral diamine / various solvent(s)

2: 85 percent / DIBAL

3: 92 percent / TsOH

4: 96 percent / mCPBA

5: 97 percent / CuI

6: 93 percent / i-Pr₂NEt

With copper(l) iodide; tin(II) trifluoromethanesulfonate; chiral diamine; tin(II) oxide; diisobutylaluminium hydride; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; In various solvent(s);
DOI:10.1016/0040-4039(94)88514-1

Reference yield:

: 117711-00-9
tridecylmagnesium bromide

: 169238-11-3
(4R,5R)-5-Benzyloxy-4-((R)-1-methoxymethoxy-pentadecyl)-2,2-dimethyl-[1,3]dioxane

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / CuI

2: 93 percent / i-Pr₂NEt

With copper(l) iodide; N-ethyl-N,N-diisopropylamine;
DOI:10.1016/0040-4039(94)88514-1