(R)-1-((4R,5R)-5-Benzyloxy-2,2-dimethyl-[1,3]dioxan-4-yl)-pentadecan-1-ol

Base Information

Chemical Name:(R)-1-((4R,5R)-5-Benzyloxy-2,2-dimethyl-[1,3]dioxan-4-yl)-pentadecan-1-ol
CAS No.:161459-71-8
Molecular Formula:C₂₈H₄₈O₄
Molecular Weight:448.687
Hs Code.:

Synonyms:(R)-1-((4R,5R)-5-Benzyloxy-2,2-dimethyl-[1,3]dioxan-4-yl)-pentadecan-1-ol

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Chemical Property of (R)-1-((4R,5R)-5-Benzyloxy-2,2-dimethyl-[1,3]dioxan-4-yl)-pentadecan-1-ol

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Technology Process of (R)-1-((4R,5R)-5-Benzyloxy-2,2-dimethyl-[1,3]dioxan-4-yl)-pentadecan-1-ol

There total 5 articles about (R)-1-((4R,5R)-5-Benzyloxy-2,2-dimethyl-[1,3]dioxan-4-yl)-pentadecan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 117711-00-9
tridecylmagnesium bromide

: 161459-70-7
(4R,5R)-5-Benzyloxy-2,2-dimethyl-4-(R)-oxiranyl-[1,3]dioxane

: 161459-71-8
(R)-1-((4R,5R)-5-Benzyloxy-2,2-dimethyl-[1,3]dioxan-4-yl)-pentadecan-1-ol

Guidance literature:: With copper(l) iodide;
DOI:10.1016/0040-4039(94)88514-1

Reference yield:

: 2-(benzyloxy)-1-(trimethylsiloxy)-1-phenoxyethylene

: 161459-71-8
(R)-1-((4R,5R)-5-Benzyloxy-2,2-dimethyl-[1,3]dioxan-4-yl)-pentadecan-1-ol

Guidance literature:: Multi-step reaction with 5 steps

1: 80 percent / Sn(OTf)2, SnO, chiral diamine / various solvent(s)

2: 85 percent / DIBAL

3: 92 percent / TsOH

4: 96 percent / mCPBA

5: 97 percent / CuI

With copper(l) iodide; tin(II) trifluoromethanesulfonate; chiral diamine; tin(II) oxide; diisobutylaluminium hydride; toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid; In various solvent(s);
DOI:10.1016/0040-4039(94)88514-1

Reference yield:

: 169276-04-4
(2R,3R)-2-Benzyloxy-pent-4-ene-1,3-diol

: 161459-71-8
(R)-1-((4R,5R)-5-Benzyloxy-2,2-dimethyl-[1,3]dioxan-4-yl)-pentadecan-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / TsOH

2: 96 percent / mCPBA

3: 97 percent / CuI

With copper(l) iodide; toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid;
DOI:10.1016/0040-4039(94)88514-1