2-benzyl-3-(4,4,5,5,-tetramethyl-1,3,2-dioxaborolan-2-yl)propanoic acid

Base Information

Chemical Name:2-benzyl-3-(4,4,5,5,-tetramethyl-1,3,2-dioxaborolan-2-yl)propanoic acid
CAS No.:1243540-17-1
Molecular Formula:C₁₆H₂₃BO₄
Molecular Weight:290.167
Hs Code.:

Synonyms:2-benzyl-3-(4,4,5,5,-tetramethyl-1,3,2-dioxaborolan-2-yl)propanoic acid

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Chemical Property of 2-benzyl-3-(4,4,5,5,-tetramethyl-1,3,2-dioxaborolan-2-yl)propanoic acid

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Technology Process of 2-benzyl-3-(4,4,5,5,-tetramethyl-1,3,2-dioxaborolan-2-yl)propanoic acid

There total 2 articles about 2-benzyl-3-(4,4,5,5,-tetramethyl-1,3,2-dioxaborolan-2-yl)propanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1243540-13-7
methyl 2-benzyl-3-(4,4,5,5,-tetramethyl-1,3,2-dioxaborolan-2-yl)propanoate

: 1243540-17-1
2-benzyl-3-(4,4,5,5,-tetramethyl-1,3,2-dioxaborolan-2-yl)propanoic acid

Guidance literature:: With water; lithium hydroxide; In tetrahydrofuran; at 20 ℃; for 1h;
DOI:10.1039/c004247a

Reference yield: 92.0%

: 1243540-13-7
methyl 2-benzyl-3-(4,4,5,5,-tetramethyl-1,3,2-dioxaborolan-2-yl)propanoate

: 7732-18-5
water

: 1243540-17-1
2-benzyl-3-(4,4,5,5,-tetramethyl-1,3,2-dioxaborolan-2-yl)propanoic acid

Guidance literature:: With LiOH; In tetrahydrofuran; H₂O; treatment of THF soln. of boron compd. with aq. soln. of LiOH at room temp. for 1 h; NMR and MS;
DOI:10.1039/c004247a

Reference yield:

: 1243540-17-1
2-benzyl-3-(4,4,5,5,-tetramethyl-1,3,2-dioxaborolan-2-yl)propanoic acid

: 29022-11-5
N-(fluoren-9-ylmethoxycarbonyl)glycine

: 35661-39-3,136132-75-7
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine

: 71989-38-3,118488-18-9,204384-67-8
Fmoc-Tyr(tBu)-OH

: 132327-80-1,200623-62-7
Fmoc-L-Gln(Trt)-OH

: 187618-60-6
Nα-(9-fluorenylmethyloxycarbonyl)-Nγ-2,2,4,6,7-pentamethyldihydrobenzofuran-5-sulfonyl-L-arginine

: (HO)2BCH₂CH(CH₂Ph)CO-Gly-Arg-Gln-Ala-Tyr

Guidance literature:: Fmoc-Tyr(tBu)-OH; With diisopropyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide; at 0 ℃;

With dmap; In N,N-dimethyl-formamide; for 0.75h; Inert atmosphere;

2-benzyl-3-(4,4,5,5,-tetramethyl-1,3,2-dioxaborolan-2-yl)propanoic acid; N-(fluoren-9-ylmethoxycarbonyl)glycine; N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine; Fmoc-L-Gln(Trt)-OH; Nα-(9-fluorenylmethyloxycarbonyl)-Nγ-2,2,4,6,7-pentamethyldihydrobenzofuran-5-sulfonyl-L-arginine; Further stages;
DOI:10.1039/c004247a