(S)-8a,9-dihydro-7-phenyl-3H-diimidazo<1,5-a:4',5'>pyridide-6,8(4H,7H)-dione

Base Information

• Chemical Name: (S)-8a,9-dihydro-7-phenyl-3H-diimidazo<1,5-a:4',5'>pyridide-6,8(4H,7H)-dione
• CAS No.: 114786-40-2
• Molecular Formula: C₁₄H₁₂N₄O₂
• Molecular Weight: 268.275

Synonyms:(S)-8a,9-dihydro-7-phenyl-3H-diimidazo<1,5-a:4',5'>pyridide-6,8(4H,7H)-dione

Chemical Property of (S)-8a,9-dihydro-7-phenyl-3H-diimidazo<1,5-a:4',5'>pyridide-6,8(4H,7H)-dione

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (S)-8a,9-dihydro-7-phenyl-3H-diimidazo<1,5-a:4',5'>pyridide-6,8(4H,7H)-dione

There total 2 articles about (S)-8a,9-dihydro-7-phenyl-3H-diimidazo<1,5-a:4',5'>pyridide-6,8(4H,7H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

phenyl isocyanate (103-71-9) + methyl (6S)-4,5,6,7-tetrahydro-1H-imidazo<4,5-c>pyridine-6-carboxylate (88932-19-8) → (S)-8a,9-dihydro-7-phenyl-3H-diimidazo<1,5-a:4',5'>pyridide-6,8(4H,7H)-dione (114786-40-2)

Guidance literature:

With triethylamine; In N,N-dimethyl-formamide; for 2h; Ambient temperature;

DOI:10.1021/jm00115a014

Reference yield: 69.0%

(6S)-4,5,6,7-tetrahydro-3H-imidazole[4,5-c]pyridine-6-carboxylic acid methyl ester (88932-19-8) + phenyl isocyanate (103-71-9) → (S)-8a,9-dihydro-7-phenyl-3H-diimidazo<1.5-a:4'.5'-d>pyridine-6,8-(4H,7H)-dione (114786-40-2)

Guidance literature:

With triethylamine; In N,N-dimethyl-formamide; for 2h; Ambient temperature;

DOI:10.1002/jhet.5570280118

Reference yield: 25.1%

benzyl bromide (100-39-0) + (S)-8a,9-dihydro-7-phenyl-3H-diimidazo<1,5-a:4',5'>pyridide-6,8(4H,7H)-dione (114786-40-2) → 8a,9-dihydro-7-phenyl-1-(phenylmethyl)-1H-diimidazo<1,5-a:4',5'-d>pyridine-6,8(4H,7H)-dione (114923-79-4) + 8a,9-dihydro-7-phenyl-3-(phenylmethyl)-3H-diimidazo<1,5-a:4',5'-d>pyridine-6,8(4H,7H)-dione (133807-95-1)

Guidance literature:

With tetramethyl ammoniumhydroxide; In methanol; N,N-dimethyl-formamide; for 0.5h;

DOI:10.1021/jm00115a014

upstream raw materials:

(6S)-4,5,6,7-tetrahydro-3H-imidazole[4,5-c]pyridine-6-carboxylic acid methyl ester

phenyl isocyanate

methyl (6S)-4,5,6,7-tetrahydro-1H-imidazo<4,5-c>pyridine-6-carboxylate

Downstream raw materials:

8a,9-dihydro-7-phenyl-3-(phenylmethyl)-1H-diimidazo<1.5-a:4'.5'-d>pyridine-6,8-(4H,7H)-dione

8a,9-dihydro-7-phenyl-1-(phenylmethyl)-1H-diimidazo<1.5-a:4'.5'-d>pyridine-6,8-(4H,7H)-dione

8a,9-dihydro-7-phenyl-1-(phenylmethyl)-1H-diimidazo<1,5-a:4',5'-d>pyridine-6,8(4H,7H)-dione

8a,9-dihydro-7-phenyl-3-(phenylmethyl)-3H-diimidazo<1,5-a:4',5'-d>pyridine-6,8(4H,7H)-dione

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 114786-40-2 (S)-8a,9-dihydro-7-phenyl-3H-diimidazo<1,5-a:4',5'>pyridide-6,8(4H,7H)-dione

Send

Send

Metric Ton KG G Pound L ML

Send

Send