O-(3aS,4S,5S,6R,7aR)-3a-benzyloxy-6-(tert-butyldimethylsilyloxymethyl)-4-methoxymethoxy-2-oxohexahydro-2H-furo[2,3-b]pyran-5-yl S-methyl carbonodithioate

Base Information

Chemical Name:O-(3aS,4S,5S,6R,7aR)-3a-benzyloxy-6-(tert-butyldimethylsilyloxymethyl)-4-methoxymethoxy-2-oxohexahydro-2H-furo[2,3-b]pyran-5-yl S-methyl carbonodithioate
CAS No.:960119-81-7
Molecular Formula:C₂₅H₃₈O₈S₂Si
Molecular Weight:558.789
Hs Code.:

O-(3aS,4S,5S,6R,7aR)-3a-benzyloxy-6-(tert-butyldimethylsilyloxymethyl)-4-methoxymethoxy-2-oxohexahydro-2H-furo[2,3-b]pyran-5-yl S-methyl carbonodithioate

Synonyms:O-(3aS,4S,5S,6R,7aR)-3a-benzyloxy-6-(tert-butyldimethylsilyloxymethyl)-4-methoxymethoxy-2-oxohexahydro-2H-furo[2,3-b]pyran-5-yl S-methyl carbonodithioate

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Chemical Property of O-(3aS,4S,5S,6R,7aR)-3a-benzyloxy-6-(tert-butyldimethylsilyloxymethyl)-4-methoxymethoxy-2-oxohexahydro-2H-furo[2,3-b]pyran-5-yl S-methyl carbonodithioate

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Technology Process of O-(3aS,4S,5S,6R,7aR)-3a-benzyloxy-6-(tert-butyldimethylsilyloxymethyl)-4-methoxymethoxy-2-oxohexahydro-2H-furo[2,3-b]pyran-5-yl S-methyl carbonodithioate

There total 1 articles about O-(3aS,4S,5S,6R,7aR)-3a-benzyloxy-6-(tert-butyldimethylsilyloxymethyl)-4-methoxymethoxy-2-oxohexahydro-2H-furo[2,3-b]pyran-5-yl S-methyl carbonodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₄H₃₆O₈S₂Si

: 74-88-4
methyl iodide

: 960119-81-7
O-(3aS,4S,5S,6R,7aR)-3a-benzyloxy-6-(tert-butyldimethylsilyloxymethyl)-4-methoxymethoxy-2-oxohexahydro-2H-furo[2,3-b]pyran-5-yl S-methyl carbonodithioate

Guidance literature:: In tetrahydrofuran; at -78 ℃;
DOI:10.1002/anie.200703027

Reference yield: 100.0%

: 960119-81-7
O-(3aS,4S,5S,6R,7aR)-3a-benzyloxy-6-(tert-butyldimethylsilyloxymethyl)-4-methoxymethoxy-2-oxohexahydro-2H-furo[2,3-b]pyran-5-yl S-methyl carbonodithioate

: 960123-55-1
(3aS,4S,6S,7aR)-3a-benzyloxy-6-(tert-butyldimethylsilyloxymethyl)-4-methoxymethoxyhexahydro-2H-furo[2,3-b]pyran-2-one

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; at 20 ℃; Inert atmosphere; Reflux;
DOI:10.1002/chem.200801103