O-benzoyl-N,N-dicyclohexylhydroxylamine

Base Information

• Chemical Name: O-benzoyl-N,N-dicyclohexylhydroxylamine
• CAS No.: 1393640-95-3
• Molecular Formula: C₁₉H₂₇NO₂
• Molecular Weight: 301.429
• Mol file: 1393640-95-3.mol

Synonyms:O-benzoyl-N,N-dicyclohexylhydroxylamine

Chemical Property of O-benzoyl-N,N-dicyclohexylhydroxylamine

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of O-benzoyl-N,N-dicyclohexylhydroxylamine

There total 1 articles about O-benzoyl-N,N-dicyclohexylhydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

N-cyclohexyl-cyclohexanamine (101-83-7) + dibenzoyl peroxide (94-36-0) → O-benzoyl-N,N-dicyclohexylhydroxylamine (1393640-95-3)

Guidance literature:

dibenzoyl peroxide; With disodium hydrogenphosphate; In N,N-dimethyl-formamide; at 20 ℃; for 3h;

N-cyclohexyl-cyclohexanamine; In N,N-dimethyl-formamide; at 20 ℃; for 21h;

DOI:10.1021/acs.joc.8b02885

Reference yield: 80.0%

triphenylboroxine (3262-89-3) + O-benzoyl-N,N-dicyclohexylhydroxylamine (1393640-95-3) → N,N-dicyclohexylbenzenamine (63302-13-6)

Guidance literature:

triphenylboroxine; With potassium carbonate; In 1,4-dioxane; at 130 ℃; for 24h; Inert atmosphere;

O-benzoyl-N,N-dicyclohexylhydroxylamine; In 1,4-dioxane; Inert atmosphere;

DOI:10.1021/ol301912a

Reference yield: 71.0%

O-benzoyl-N,N-dicyclohexylhydroxylamine (1393640-95-3) + dibenzoyl peroxide (94-36-0) → N-benzoylcyclohexylamine (1759-68-8)

Guidance literature:

With triethyl phosphite; In 1,2-dichloro-ethane; at 85 ℃; for 24h;

DOI:10.1002/ejoc.202000611

upstream raw materials:

N-cyclohexyl-cyclohexanamine

dibenzoyl peroxide

Downstream raw materials:

N,N-dicyclohexylbenzenamine

N-benzoylcyclohexylamine