Mo⁽²⁺⁾*NO⁽¹⁺⁾*S(CH₂CH₂SC₆H₂(C(CH₃)3)2S)2^(2-)*BF₄^(1-)=[Mo(NO)(S(CH₂CH₂SC₆H₂(C(CH₃)3)2S)2)]BF₄

Base Information

• Chemical Name: Mo⁽²⁺⁾*NO⁽¹⁺⁾*S(CH₂CH₂SC₆H₂(C(CH₃)3)2S)2^(2-)*BF₄^(1-)=[Mo(NO)(S(CH₂CH₂SC₆H₂(C(CH₃)3)2S)2)]BF₄
• CAS No.: 170892-49-6
• Molecular Formula: BF₄*C₃₂H₄₈S₅*Mo*NO
• Molecular Weight: 805.814

Synonyms:Mo⁽²⁺⁾*NO⁽¹⁺⁾*S(CH₂CH₂SC₆H₂(C(CH₃)3)2S)2^(2-)*BF₄^(1-)=[Mo(NO)(S(CH₂CH₂SC₆H₂(C(CH₃)3)2S)2)]BF₄

Chemical Property of Mo⁽²⁺⁾*NO⁽¹⁺⁾*S(CH₂CH₂SC₆H₂(C(CH₃)3)2S)2^(2-)*BF₄^(1-)=[Mo(NO)(S(CH₂CH₂SC₆H₂(C(CH₃)3)2S)2)]BF₄

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Technology Process of Mo⁽²⁺⁾*NO⁽¹⁺⁾*S(CH₂CH₂SC₆H₂(C(CH₃)3)2S)2^(2-)*BF₄^(1-)=[Mo(NO)(S(CH₂CH₂SC₆H₂(C(CH₃)3)2S)2)]BF₄

There total 3 articles about Mo⁽²⁺⁾*NO⁽¹⁺⁾*S(CH₂CH₂SC₆H₂(C(CH₃)3)2S)2^(2-)*BF₄^(1-)=[Mo(NO)(S(CH₂CH₂SC₆H₂(C(CH₃)3)2S)2)]BF₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

Mo(2+)*2CO*S(CH2CH2SC6H2(C(CH3)3)2S)2(2-)=Mo(CO)2(S(CH2CH2SC6H2(C(CH3)3)2S)2) + nitrosonium tetrafluoroborate → Mo(2+)*NO(1+)*S(CH2CH2SC6H2(C(CH3)3)2S)2(2-)*BF4(1-)=[Mo(NO)(S(CH2CH2SC6H2(C(CH3)3)2S)2)]BF4 (170892-49-6)

Guidance literature:

In dichloromethane; byproducts: CO; N2-atmosphere; addn. of slight excess of NOBF4 to Mo-complex suspn. (room temp.); evapn., stirring with hexane, filtration, washing (hexane), drying (vac.); elem. anal.;

DOI:10.1021/ic00128a006

Reference yield:

Mo(2+)*NO(1+)*N3(1-)*S(CH2CH2SC6H2(C(CH3)3)2S)2(2-)=Mo(NO)(N3)(S(CH2CH2SC6H2(C(CH3)3)2S)2) + nitrosonium tetrafluoroborate → hydrogen azide (7782-79-8) + Mo(2+)*NO(1+)*S(CH2CH2SC6H2(C(CH3)3)2S)2(2-)*BF4(1-)=[Mo(NO)(S(CH2CH2SC6H2(C(CH3)3)2S)2)]BF4 (170892-49-6) + dinitrogen monoxide (10024-97-2)

Guidance literature:

In tetrahydrofuran; N2-atmosphere; not isolated, reaction followed by IR spectroscopy;

DOI:10.1021/ic00128a006

Reference yield:

tetrafluoroboric acid + Mo(2+)*NO(1+)*N3(1-)*S(CH2CH2SC6H2(C(CH3)3)2S)2(2-)=Mo(NO)(N3)(S(CH2CH2SC6H2(C(CH3)3)2S)2) → hydrogen azide (7782-79-8) + Mo(2+)*NO(1+)*S(CH2CH2SC6H2(C(CH3)3)2S)2(2-)*BF4(1-)=[Mo(NO)(S(CH2CH2SC6H2(C(CH3)3)2S)2)]BF4 (170892-49-6)

Guidance literature:

In tetrahydrofuran; N2-atmosphere; not isolated, reaction followed by IR spectroscopy;

DOI:10.1021/ic00128a006

Downstream raw materials:

Mo⁽²⁺⁾*NO⁽¹⁺⁾*S(CH₂CH₂SC₆H₂(C(CH₃)3)2S)2^(2-)=[Mo(NO)(S(CH₂CH₂SC₆H₂(C(CH₃)3)2S)2)]⁽¹⁺⁾

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