C₆₇H₇₄Cl₃N₅O₁₅

Base Information

Chemical Name:C₆₇H₇₄Cl₃N₅O₁₅
CAS No.:215029-91-7
Molecular Formula:C₆₇H₇₄Cl₃N₅O₁₅
Molecular Weight:1295.71
Hs Code.:

C<sub>67</sub>H<sub>74</sub>Cl<sub>3</sub>N<sub>5</sub>O<sub>15</sub>

Synonyms:C₆₇H₇₄Cl₃N₅O₁₅

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₆₇H₇₄Cl₃N₅O₁₅

Chemical Property:

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Technology Process of C₆₇H₇₄Cl₃N₅O₁₅

There total 8 articles about C₆₇H₇₄Cl₃N₅O₁₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 545-06-2
trichloroacetonitrile

: C₆₅H₇₄N₄O₁₅

: 215029-91-7
C₆₇H₇₄Cl₃N₅O₁₅

Guidance literature:: With potassium carbonate; In dichloromethane; Ambient temperature;
DOI:10.1021/ja980724z

Reference yield:

: 114117-12-3
2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl-(1->4)-1,5-anhydro-2-deoxy-3,6-di-O-benzyl-D-arabino-hex-1-enitol

: 215029-91-7
C₆₇H₇₄Cl₃N₅O₁₅

Guidance literature:: Multi-step reaction with 8 steps

1: 90 percent / I(sym-collidine)2ClO₄, 4A molecular sieves / CH₂Cl₂ / 0.25 h / 0 °C

2: 1.) LiHMDS / 1.) DMF, -40 deg C, 15 min, 2.) DMF, -40 deg C, 4 h

3: 84 percent / di-tert-butylpyridine, MeOTf, 4A molecular sieves / CH₂Cl₂; diethyl ether / 5 h / 0 °C

4: pyridine, DMAP / 0 - 20 °C

5: Na/Hg, aq. Na₂HPO₄ / methanol; ethyl acetate / 2 h / Ambient temperature

6: 27 percent / NaN₃, CAN / acetonitrile / 4 h / -40 °C

7: 170 mg / EtN(i-Pr)2, PhSH / acetonitrile / 0.5 h / Ambient temperature

8: 42 percent / K₂CO₃ / CH₂Cl₂ / Ambient temperature

With pyridine; dmap; disodium hydrogenphosphate; sodium amalgam; sodium azide; ammonium cerium(IV) nitrate; iodonium(di-γ-collidine) perchlorate; 4 A molecular sieve; potassium carbonate; thiophenol; N-ethyl-N,N-diisopropylamine; Di-tert-butylpyridine; methyl trifluoromethanesulfonate; lithium hexamethyldisilazane; In methanol; diethyl ether; dichloromethane; ethyl acetate; acetonitrile;
DOI:10.1021/ja980724z

Reference yield:

: 213331-84-1
N-[(2S,3R,4R,5S,6R)-4-Benzyloxy-6-benzyloxymethyl-2-ethylsulfanyl-5-((2S,3R,4S,5S,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-3-yl]-benzenesulfonamide

: 215029-91-7
C₆₇H₇₄Cl₃N₅O₁₅

Guidance literature:: Multi-step reaction with 6 steps

1: 84 percent / di-tert-butylpyridine, MeOTf, 4A molecular sieves / CH₂Cl₂; diethyl ether / 5 h / 0 °C

2: pyridine, DMAP / 0 - 20 °C

3: Na/Hg, aq. Na₂HPO₄ / methanol; ethyl acetate / 2 h / Ambient temperature

4: 27 percent / NaN₃, CAN / acetonitrile / 4 h / -40 °C

5: 170 mg / EtN(i-Pr)2, PhSH / acetonitrile / 0.5 h / Ambient temperature

6: 42 percent / K₂CO₃ / CH₂Cl₂ / Ambient temperature

With pyridine; dmap; disodium hydrogenphosphate; sodium amalgam; sodium azide; ammonium cerium(IV) nitrate; 4 A molecular sieve; potassium carbonate; thiophenol; N-ethyl-N,N-diisopropylamine; Di-tert-butylpyridine; methyl trifluoromethanesulfonate; In methanol; diethyl ether; dichloromethane; ethyl acetate; acetonitrile;
DOI:10.1021/ja980724z