C₆₆H₁₀₂S₃

Base Information

Chemical Name:C₆₆H₁₀₂S₃
CAS No.:791849-55-3
Molecular Formula:C₆₆H₁₀₂S₃
Molecular Weight:991.734
Hs Code.:

C<sub>66</sub>H<sub>102</sub>S<sub>3</sub>

Synonyms:C₆₆H₁₀₂S₃

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Chemical Property of C₆₆H₁₀₂S₃

Chemical Property:

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Technology Process of C₆₆H₁₀₂S₃

There total 7 articles about C₆₆H₁₀₂S₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 51329-15-8
methyl 3,5-dibromobenzoate

: 791849-55-3
C₆₆H₁₀₂S₃

Guidance literature:: Multi-step reaction with 6 steps

1: 85 percent / Pd(PPh₃)2Cl₂; copper(I) iodide; triethylamine / benzene / 48 h / 80 °C

2: 95 percent / H₂ / Pd/C / ethanol / 18 h / 25 °C / atmospheric pressure

3: 95 percent / LiAlH₄ / tetrahydrofuran / 1 h / 25 °C

4: 87 percent / diisopropyl azodicarboxylate; PPh₃ / tetrahydrofuran / 2 h / 25 °C

5: sodium methoxide / tetrahydrofuran; methanol / 0.08 h / 25 °C

6: 1.48 g / methanol; tetrahydrofuran / 1 h / 25 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; lithium aluminium tetrahydride; di-isopropyl azodicarboxylate; hydrogen; sodium methylate; triethylamine; triphenylphosphine; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; benzene; 1: Sonogashira coupling / 4: Mitsunobu reaction;
DOI:10.1021/ja046557m

Reference yield:

: 693-02-7
hex-1-yne

: 791849-55-3
C₆₆H₁₀₂S₃

Guidance literature:: Multi-step reaction with 6 steps

1: 85 percent / Pd(PPh₃)2Cl₂; copper(I) iodide; triethylamine / benzene / 48 h / 80 °C

2: 95 percent / H₂ / Pd/C / ethanol / 18 h / 25 °C / atmospheric pressure

3: 95 percent / LiAlH₄ / tetrahydrofuran / 1 h / 25 °C

4: 87 percent / diisopropyl azodicarboxylate; PPh₃ / tetrahydrofuran / 2 h / 25 °C

5: sodium methoxide / tetrahydrofuran; methanol / 0.08 h / 25 °C

6: 1.48 g / methanol; tetrahydrofuran / 1 h / 25 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; lithium aluminium tetrahydride; di-isopropyl azodicarboxylate; hydrogen; sodium methylate; triethylamine; triphenylphosphine; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; benzene; 1: Sonogashira coupling / 4: Mitsunobu reaction;
DOI:10.1021/ja046557m

Reference yield:

: 791849-42-8
methyl 3,5-di(hex-1-ynyl)benzoate

: 791849-55-3
C₆₆H₁₀₂S₃

Guidance literature:: Multi-step reaction with 5 steps

1: 95 percent / H₂ / Pd/C / ethanol / 18 h / 25 °C / atmospheric pressure

2: 95 percent / LiAlH₄ / tetrahydrofuran / 1 h / 25 °C

3: 87 percent / diisopropyl azodicarboxylate; PPh₃ / tetrahydrofuran / 2 h / 25 °C

4: sodium methoxide / tetrahydrofuran; methanol / 0.08 h / 25 °C

5: 1.48 g / methanol; tetrahydrofuran / 1 h / 25 °C

With lithium aluminium tetrahydride; di-isopropyl azodicarboxylate; hydrogen; sodium methylate; triphenylphosphine; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; 3: Mitsunobu reaction;
DOI:10.1021/ja046557m