3-[bis(4-methoxyphenyl)methyl]-4-methyl-1,2,3-oxathiazolidine-4-carboxylic acid tert-butyl ester 2,2-dioxide

Base Information

Chemical Name:3-[bis(4-methoxyphenyl)methyl]-4-methyl-1,2,3-oxathiazolidine-4-carboxylic acid tert-butyl ester 2,2-dioxide
CAS No.:438574-31-3
Molecular Formula:C₂₃H₂₉NO₇S
Molecular Weight:463.552
Hs Code.:

Synonyms:3-[bis(4-methoxyphenyl)methyl]-4-methyl-1,2,3-oxathiazolidine-4-carboxylic acid tert-butyl ester 2,2-dioxide

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Chemical Property of 3-[bis(4-methoxyphenyl)methyl]-4-methyl-1,2,3-oxathiazolidine-4-carboxylic acid tert-butyl ester 2,2-dioxide

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Technology Process of 3-[bis(4-methoxyphenyl)methyl]-4-methyl-1,2,3-oxathiazolidine-4-carboxylic acid tert-butyl ester 2,2-dioxide

There total 5 articles about 3-[bis(4-methoxyphenyl)methyl]-4-methyl-1,2,3-oxathiazolidine-4-carboxylic acid tert-butyl ester 2,2-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 438574-29-9
3-[bis(4-methoxyphenyl)methyl]-4-methyl-1,2,3-oxathiazolidine-4-carboxylic acid tert-butyl ester 2-oxide

: 438574-31-3
3-[bis(4-methoxyphenyl)methyl]-4-methyl-1,2,3-oxathiazolidine-4-carboxylic acid tert-butyl ester 2,2-dioxide

Guidance literature:: With ruthenium(IV) oxide; sodium periodate; In acetonitrile;
DOI:10.1021/jm010241x

Reference yield:

: 438574-22-2
3-benzyloxy-2-[N-(tert-butoxycarbonyl)amino]-2-methylpropanoic acid tert-butyl ester

: 438574-31-3
3-[bis(4-methoxyphenyl)methyl]-4-methyl-1,2,3-oxathiazolidine-4-carboxylic acid tert-butyl ester 2,2-dioxide

Guidance literature:: Multi-step reaction with 5 steps

1: 100 percent / H₂ / 10percent Pd/C / methanol

2: p-TsOH*H₂O / diethyl ether; ethanol

3: Et₃N / CH₂Cl₂ / 1 h / 20 °C

4: 83 percent / Et₃N; SOCl₂ / toluene

5: 89 percent / NaIO₄; aq. RuO₂ / acetonitrile

With ruthenium(IV) oxide; sodium periodate; thionyl chloride; hydrogen; toluene-4-sulfonic acid; triethylamine; 10percent Pd/C; In methanol; diethyl ether; ethanol; dichloromethane; toluene; acetonitrile;
DOI:10.1021/jm010241x

Reference yield:

: 438574-27-7
3-hydroxy-2-(N-[bis(4-methoxyphenyl)methyl]amino)-2-methylpropanoic acid tert-butyl ester

: 438574-31-3
3-[bis(4-methoxyphenyl)methyl]-4-methyl-1,2,3-oxathiazolidine-4-carboxylic acid tert-butyl ester 2,2-dioxide

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / Et₃N; SOCl₂ / toluene

2: 89 percent / NaIO₄; aq. RuO₂ / acetonitrile

With ruthenium(IV) oxide; sodium periodate; thionyl chloride; triethylamine; In toluene; acetonitrile;
DOI:10.1021/jm010241x