2-benzyloxy-6-(4-tert-butoxycarbonylamino-butoxy)-benzoic acid methyl ester

Base Information

Chemical Name:2-benzyloxy-6-(4-tert-butoxycarbonylamino-butoxy)-benzoic acid methyl ester
CAS No.:952339-49-0
Molecular Formula:C₂₄H₃₁NO₆
Molecular Weight:429.513
Hs Code.:

Synonyms:2-benzyloxy-6-(4-tert-butoxycarbonylamino-butoxy)-benzoic acid methyl ester

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Chemical Property of 2-benzyloxy-6-(4-tert-butoxycarbonylamino-butoxy)-benzoic acid methyl ester

Chemical Property:

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Technology Process of 2-benzyloxy-6-(4-tert-butoxycarbonylamino-butoxy)-benzoic acid methyl ester

There total 1 articles about 2-benzyloxy-6-(4-tert-butoxycarbonylamino-butoxy)-benzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-39-0
benzyl bromide

: 436864-52-7
2-(4-tert-butoxycarbonylaminobutoxy)-6-hydroxybenzoic acid methyl ester

: 952339-49-0
2-benzyloxy-6-(4-tert-butoxycarbonylamino-butoxy)-benzoic acid methyl ester

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 3h;

Reference yield:

: 952339-49-0
2-benzyloxy-6-(4-tert-butoxycarbonylamino-butoxy)-benzoic acid methyl ester

: 623563-64-4
2-(4-aminobutoxy)-6-benzyloxybenzoic acid methyl ester

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 0.333333h;

Reference yield:

: 952339-49-0
2-benzyloxy-6-(4-tert-butoxycarbonylamino-butoxy)-benzoic acid methyl ester

: 2-(4-{3-[3-fluoro-5-hydroxy-4-(1,1,4-trioxo-[1,2,5]thiadiazolidin-2-yl)-phenyl]-propionylamino}-butoxy)-6-hydroxy-benzoic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: trifluoroacetic acid / dichloromethane / 0.33 h / 20 °C

2.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 0.17 h / 20 °C

2.2: 18 h / 20 °C

3.1: hydrogen; potassium carbonate / palladium 10% on activated carbon / ethanol; water / 2 h / 760.05 Torr

With hydrogen; potassium carbonate; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; palladium 10% on activated carbon; In ethanol; dichloromethane; water; N,N-dimethyl-formamide;