N-(ethoxycarbonyl)-3-exo-phenyl-6-(phenylselenenyl)-2-azabicyclo<2.2.2>oct-5-ene

Base Information

• Chemical Name: N-(ethoxycarbonyl)-3-exo-phenyl-6-(phenylselenenyl)-2-azabicyclo<2.2.2>oct-5-ene
• CAS No.: 113777-78-9
• Molecular Formula: C₂₂H₂₃NO₂Se
• Molecular Weight: 412.39

Synonyms:N-(ethoxycarbonyl)-3-exo-phenyl-6-(phenylselenenyl)-2-azabicyclo<2.2.2>oct-5-ene

Chemical Property of N-(ethoxycarbonyl)-3-exo-phenyl-6-(phenylselenenyl)-2-azabicyclo<2.2.2>oct-5-ene

Chemical Property:

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Technology Process of N-(ethoxycarbonyl)-3-exo-phenyl-6-(phenylselenenyl)-2-azabicyclo<2.2.2>oct-5-ene

There total 3 articles about N-(ethoxycarbonyl)-3-exo-phenyl-6-(phenylselenenyl)-2-azabicyclo<2.2.2>oct-5-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Phenylselenyl chloride (5707-04-0) → N-(ethoxycarbonyl)-3-exo-phenyl-6-(phenylselenenyl)-2-azabicyclo<2.2.2>oct-5-ene (113777-78-9)

Guidance literature:

Multi-step reaction with 2 steps

1: CH₂Cl₂ / 13 h / Ambient temperature

2: DBU / 15 h / Heating

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane;

DOI:10.1021/jo00245a024

Reference yield:

(1S,3S,4R)-3-Phenyl-2-aza-bicyclo[2.2.2]oct-5-ene-2-carboxylic acid ethyl ester (113830-06-1) → N-(ethoxycarbonyl)-3-exo-phenyl-6-(phenylselenenyl)-2-azabicyclo<2.2.2>oct-5-ene (113777-78-9)

Guidance literature:

Multi-step reaction with 2 steps

1: CH₂Cl₂ / 13 h / Ambient temperature

2: DBU / 15 h / Heating

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane;

DOI:10.1021/jo00245a024

Reference yield:

(1S,3S,4S)-5-Chloro-3-phenyl-6-phenylselanyl-2-aza-bicyclo[2.2.2]octane-2-carboxylic acid ethyl ester → N-(ethoxycarbonyl)-3-exo-phenyl-6-(phenylselenenyl)-2-azabicyclo<2.2.2>oct-5-ene (113777-78-9)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; for 15h; Yield given; Heating;

DOI:10.1021/jo00245a024

upstream raw materials:

Phenylselenyl chloride

(1S,3S,4R)-3-Phenyl-2-aza-bicyclo[2.2.2]oct-5-ene-2-carboxylic acid ethyl ester

Downstream raw materials:

N-(ethoxycarbonyl)-3-exo-phenyl-2-azabicyclo<2.2.2>octan-6-one

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