3-[3',5'-Bis[3''-[bis(3''',5'''-dibenzyloxy)benzyl]propoxy]benzyloxy]propanol

Base Information

Chemical Name:3-[3',5'-Bis[3''-[bis(3''',5'''-dibenzyloxy)benzyl]propoxy]benzyloxy]propanol
CAS No.:244207-18-9
Molecular Formula:C₅₈H₆₂O₁₀
Molecular Weight:919.124
Hs Code.:

Synonyms:3-[3',5'-Bis[3''-[bis(3''',5'''-dibenzyloxy)benzyl]propoxy]benzyloxy]propanol

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Chemical Property of 3-[3',5'-Bis[3''-[bis(3''',5'''-dibenzyloxy)benzyl]propoxy]benzyloxy]propanol

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Technology Process of 3-[3',5'-Bis[3''-[bis(3''',5'''-dibenzyloxy)benzyl]propoxy]benzyloxy]propanol

There total 7 articles about 3-[3',5'-Bis[3''-[bis(3''',5'''-dibenzyloxy)benzyl]propoxy]benzyloxy]propanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 244207-17-8
Allyl 3,5-bis[3'-[3'',5''-(dibenzyloxy)benzyloxy]propoxy]benzyl ether

: 244207-18-9
3-[3',5'-Bis[3''-[bis(3''',5'''-dibenzyloxy)benzyl]propoxy]benzyloxy]propanol

Guidance literature:: Allyl 3,5-bis[3'-[3'',5''-(dibenzyloxy)benzyloxy]propoxy]benzyl ether; With 9-borabicyclo[3.3.1]nonane dimer; In tetrahydrofuran; at 20 ℃; for 14h;

With sodium hydroxide; water; dihydrogen peroxide; In tetrahydrofuran; ethanol; at 50 ℃; for 3h;
DOI:10.1002/(SICI)1521-3765(19990802)5:8<2362::AID-CHEM2362>3.0.CO;2-5

Reference yield:

: 24131-31-5
3,5-dibenzyloxybenzyl alcohol

: 244207-18-9
3-[3',5'-Bis[3''-[bis(3''',5'''-dibenzyloxy)benzyl]propoxy]benzyloxy]propanol

Guidance literature:: Multi-step reaction with 6 steps

1.1: NaH / tetrahydrofuran / 0.5 h / Heating

1.2: 98 percent / tetrahydrofuran / 24 h / Heating

2.1: 9-BBN / tetrahydrofuran / 14 h / 20 °C

2.2: 90 percent / H₂O₂; NaOH; H₂O / tetrahydrofuran; ethanol / 3 h / 50 °C

3.1: 94 percent / Ph₃P; CBr₄ / tetrahydrofuran / 1.33 h / 20 °C

4.1: 97 percent / K₂CO₃; [18]crown-6 / acetone / 72 h / Heating

5.1: NaH / tetrahydrofuran / Heating

5.2: 96 percent / tetrahydrofuran / Heating

6.1: 9-BBN / tetrahydrofuran / 14 h / 20 °C

6.2: 87 percent / H₂O₂; NaOH; H₂O / tetrahydrofuran; ethanol / 3 h / 50 °C

With 9-borabicyclo[3.3.1]nonane dimer; 18-crown-6 ether; carbon tetrabromide; sodium hydride; potassium carbonate; triphenylphosphine; In tetrahydrofuran; acetone; 1.1: Metallation / 1.2: Etherification / 2.1: Addition / 2.2: Oxidation / 3.1: Substitution / 4.1: Etherification / 5.1: Metallation / 5.2: Etherification / 6.1: Addition / 6.2: Oxidation;
DOI:10.1002/(SICI)1521-3765(19990802)5:8<2362::AID-CHEM2362>3.0.CO;2-5

Reference yield:

: 29654-55-5
5-(hydroxymethyl)benzene-1,3-diol

: 244207-18-9
3-[3',5'-Bis[3''-[bis(3''',5'''-dibenzyloxy)benzyl]propoxy]benzyloxy]propanol

Guidance literature:: Multi-step reaction with 3 steps

1.1: 97 percent / K₂CO₃; [18]crown-6 / acetone / 72 h / Heating

2.1: NaH / tetrahydrofuran / Heating

2.2: 96 percent / tetrahydrofuran / Heating

3.1: 9-BBN / tetrahydrofuran / 14 h / 20 °C

3.2: 87 percent / H₂O₂; NaOH; H₂O / tetrahydrofuran; ethanol / 3 h / 50 °C

With 9-borabicyclo[3.3.1]nonane dimer; 18-crown-6 ether; sodium hydride; potassium carbonate; In tetrahydrofuran; acetone; 1.1: Etherification / 2.1: Metallation / 2.2: Etherification / 3.1: Addition / 3.2: Oxidation;
DOI:10.1002/(SICI)1521-3765(19990802)5:8<2362::AID-CHEM2362>3.0.CO;2-5