2-phenylspiroinden>-1'(3'H)-one

Base Information

• Chemical Name: 2-phenylspiroinden>-1'(3'H)-one
• CAS No.: 114183-89-0
• Molecular Formula: C₁₇H₁₄O
• Molecular Weight: 234.298

Synonyms:2-phenylspiroinden>-1'(3'H)-one

Chemical Property of 2-phenylspiroinden>-1'(3'H)-one

Chemical Property:

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Technology Process of 2-phenylspiroinden>-1'(3'H)-one

There total 3 articles about 2-phenylspiroinden>-1'(3'H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.2%

trans-4',5'-dihydro-4'-phenylspiropyrazol>-1-one (138421-76-8,145411-98-9) → C17H14O (114183-89-0,138422-02-3) + Z-2-(α-methylbenzylidene)-1-indanone (138421-93-9) + E-2-(α-methylbenzylidene)-1-indanone (138421-84-8)

Guidance literature:

In neat (no solvent); for 0.5h; Yields of byproduct given; Heating;

DOI:10.1016/S0040-4020(01)91007-5

Reference yield: 59.0%

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + 2-diazo-indan-1-one (1775-23-1) → 2-phenylspiroinden>-1'(3'H)-one (114183-89-0)

Guidance literature:

With rhodium(II) acetate; In toluene; at 20 - 25 ℃;

DOI:10.1021/jo00247a007

Reference yield: 36.0%

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + 2-diazo-indan-1-one (1775-23-1) → C17H14O (114183-89-0,138422-02-3) + C17H14O

Guidance literature:

dirhodium tetraacetate; In dichloromethane; at 20 ℃; for 2h;

DOI:10.1016/S0040-4039(00)00002-2

upstream raw materials:

trans-4',5'-dihydro-4'-phenylspiropyrazol>-1-one

styrene

2-diazo-indan-1-one

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