2-(trimethylsilyl)ethyl 2,6-di-O-benzoyl-4-O-(2,6-di-O-benzoyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-β-D-glucopyranoside

Base Information

Chemical Name:2-(trimethylsilyl)ethyl 2,6-di-O-benzoyl-4-O-(2,6-di-O-benzoyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-β-D-glucopyranoside
CAS No.:151069-92-0
Molecular Formula:C₄₈H₅₄O₁₅Si
Molecular Weight:899.033
Hs Code.:

Synonyms:2-(trimethylsilyl)ethyl 2,6-di-O-benzoyl-4-O-(2,6-di-O-benzoyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-β-D-glucopyranoside

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Chemical Property of 2-(trimethylsilyl)ethyl 2,6-di-O-benzoyl-4-O-(2,6-di-O-benzoyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-β-D-glucopyranoside

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Technology Process of 2-(trimethylsilyl)ethyl 2,6-di-O-benzoyl-4-O-(2,6-di-O-benzoyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-β-D-glucopyranoside

There total 2 articles about 2-(trimethylsilyl)ethyl 2,6-di-O-benzoyl-4-O-(2,6-di-O-benzoyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 98-88-4
benzoyl chloride

: 117253-40-4
2-(trimethylsilyl)ethyl 4-O-(3,4-O-isopropylidene-β-D-galactopyranosyl)-β-D-glucopyranoside

: 151069-92-0
2-(trimethylsilyl)ethyl 2,6-di-O-benzoyl-4-O-(2,6-di-O-benzoyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-β-D-glucopyranoside

: C₅₅H₅₈O₁₆Si

Guidance literature:: With pyridine; at -45 ℃; for 4h;
DOI:10.1016/0008-6215(93)84013-V

Reference yield: 42.3%

: 151069-92-0
2-(trimethylsilyl)ethyl 2,6-di-O-benzoyl-4-O-(2,6-di-O-benzoyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-β-D-glucopyranoside

Guidance literature:

Reference yield: 29.0%

: 151069-92-0
2-(trimethylsilyl)ethyl 2,6-di-O-benzoyl-4-O-(2,6-di-O-benzoyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-β-D-glucopyranoside

: 2,3,4-tri-O-benzyl-α-L-fucopyranosyl fluoride

: C₇₅H₈₂O₁₉Si

Guidance literature:: With 4 A molecular sieve; lithium perchlorate; cesium fluoride; In diethyl ether; at 25 ℃; for 24h;
DOI:10.1016/0040-4039(95)00637-R