C₆₀H₁₀₂O₅Si₄

Base Information

Chemical Name:C₆₀H₁₀₂O₅Si₄
CAS No.:124469-37-0
Molecular Formula:C₆₀H₁₀₂O₅Si₄
Molecular Weight:1015.81
Hs Code.:

C<sub>60</sub>H<sub>102</sub>O<sub>5</sub>Si<sub>4</sub>

Synonyms:C₆₀H₁₀₂O₅Si₄

Suppliers and Price of C₆₀H₁₀₂O₅Si₄

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₆₀H₁₀₂O₅Si₄

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₆₀H₁₀₂O₅Si₄

There total 16 articles about C₆₀H₁₀₂O₅Si₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: C₆₀H₁₀₄O₄Si₄

: 124469-37-0
C₆₀H₁₀₂O₅Si₄

Guidance literature:: With 3,5-dimethyl-1H-pyrazole; chromium(VI) oxide; In dichloromethane; at -20 - -10 ℃; for 4h;
DOI:10.1016/S0040-4039(01)93715-3

Reference yield:

: 69739-34-0
t-butyldimethylsiyl triflate

: 124469-37-0
C₆₀H₁₀₂O₅Si₄

Guidance literature:: Multi-step reaction with 7 steps

1: 89 percent / 2,6-lutidine / CH₂Cl₂ / 0.17 h / 0 °C

2: 85 percent / H₂O₂ (30percent), NaOH (4 M) / 2-methyl-propan-2-ol; tetrahydrofuran / 1 h / Ambient temperature

3: 90 percent / LDA / tetrahydrofuran / 0.5 h / 0 °C

4: 93 percent / tetrahydrofuran / 0.5 h / 0 deg C to room temp.

5: 92 percent / H₂ / PtO₂ / ethyl acetate / 12 h / Ambient temperature

6: 89 percent / 2,6-lutidine / CH₂Cl₂ / 0.08 h / 0 °C

7: 71 percent / 3,5-dimethylpyrazole/CrO₃ / CH₂Cl₂ / 4 h / -20 - -10 °C

With 2,6-dimethylpyridine; 3,5-dimethyl-1H-pyrazole; chromium(VI) oxide; sodium hydroxide; hydrogen; dihydrogen peroxide; lithium diisopropyl amide; platinum(IV) oxide; In tetrahydrofuran; dichloromethane; ethyl acetate; tert-butyl alcohol;
DOI:10.1016/S0040-4039(01)93715-3

Reference yield:

: 382-45-6
adrenosterone

: 124469-37-0
C₆₀H₁₀₂O₅Si₄

Guidance literature:: Multi-step reaction with 15 steps

1: 92 percent / acetic anhydride / 6 h / Heating

2: 83 percent / p-TsOH, HC(OEt)3 / 1 h / Heating

3: 88 percent / NaBH₄ / 2-methyl-propan-2-ol; tetrahydrofuran; H₂O / 5 h / 0 deg C to room temp.

4: 95 percent / pyridine / 4 h / Ambient temperature

5: 1.) PCC; 2.) Li/liq. NH₃ / 1.) CH₂Cl₂, room temp., 2 h; 2.) dioxane, MeOH, -30 deg C

6: 94 percent / pyridine / 8 h / Ambient temperature

7: 94 percent / Br₂-HBr / pyridine; tetrahydrofuran / 2 h / Ambient temperature

8: 1.) t-BuOK; 2.) PPTS / 1.) DMSO, 40 deg C, 24 h; 2.) acetone/H₂O, room temp., 24 h

9: 89 percent / 2,6-lutidine / CH₂Cl₂ / 0.17 h / 0 °C

10: 85 percent / H₂O₂ (30percent), NaOH (4 M) / 2-methyl-propan-2-ol; tetrahydrofuran / 1 h / Ambient temperature

11: 90 percent / LDA / tetrahydrofuran / 0.5 h / 0 °C

12: 93 percent / tetrahydrofuran / 0.5 h / 0 deg C to room temp.

13: 92 percent / H₂ / PtO₂ / ethyl acetate / 12 h / Ambient temperature

14: 89 percent / 2,6-lutidine / CH₂Cl₂ / 0.08 h / 0 °C

15: 71 percent / 3,5-dimethylpyrazole/CrO₃ / CH₂Cl₂ / 4 h / -20 - -10 °C

With 2,6-dimethylpyridine; 3,5-dimethyl-1H-pyrazole; chromium(VI) oxide; sodium hydroxide; sodium tetrahydroborate; potassium tert-butylate; ammonia; hydrogen bromide; hydrogen; dihydrogen peroxide; bromine; pyridinium p-toluenesulfonate; lithium; toluene-4-sulfonic acid; orthoformic acid triethyl ester; pyridinium chlorochromate; lithium diisopropyl amide; platinum(IV) oxide; In tetrahydrofuran; pyridine; dichloromethane; water; acetic anhydride; ethyl acetate; tert-butyl alcohol;
DOI:10.1016/S0040-4039(01)93715-3