(1R,5S,9R)-3-Benzyl-1-methoxymethoxymethyl-5-methyl-3-aza-bicyclo[3.3.1]nonan-9-ol

Base Information

Chemical Name:(1R,5S,9R)-3-Benzyl-1-methoxymethoxymethyl-5-methyl-3-aza-bicyclo[3.3.1]nonan-9-ol
CAS No.:128466-30-8
Molecular Formula:C₁₉H₂₉NO₃
Molecular Weight:319.444
Hs Code.:

Synonyms:(1R,5S,9R)-3-Benzyl-1-methoxymethoxymethyl-5-methyl-3-aza-bicyclo[3.3.1]nonan-9-ol

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Chemical Property of (1R,5S,9R)-3-Benzyl-1-methoxymethoxymethyl-5-methyl-3-aza-bicyclo[3.3.1]nonan-9-ol

Chemical Property:

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Technology Process of (1R,5S,9R)-3-Benzyl-1-methoxymethoxymethyl-5-methyl-3-aza-bicyclo[3.3.1]nonan-9-ol

There total 8 articles about (1R,5S,9R)-3-Benzyl-1-methoxymethoxymethyl-5-methyl-3-aza-bicyclo[3.3.1]nonan-9-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 128466-29-5
(1R,5S,9R)-3-Benzyl-1-hydroxymethyl-5-methyl-3-aza-bicyclo[3.3.1]nonan-9-ol

: 107-30-2
chloromethyl methyl ether

: 128466-30-8
(1R,5S,9R)-3-Benzyl-1-methoxymethoxymethyl-5-methyl-3-aza-bicyclo[3.3.1]nonan-9-ol

Guidance literature:: With N-ethyl-N,N-diisopropylamine; at 0 ℃;

Reference yield:

: 128466-23-9
(1R,5S,9S)-3-Benzyl-1,5-bis-hydroxymethyl-3-aza-bicyclo[3.3.1]nonan-9-ol

: 128466-30-8
(1R,5S,9R)-3-Benzyl-1-methoxymethoxymethyl-5-methyl-3-aza-bicyclo[3.3.1]nonan-9-ol

Guidance literature:: Multi-step reaction with 7 steps

1: (+)-10-camphorsulfonic acid / benzene / Heating

2: Et₃N, DMAP

3: 97 percent / KOH / ethanol

4: DMSO, (COCl)2, Et₃N

5: 68 percent / NH₂NH₂*H₂O, NaOH / various solvent(s)

6: 92 percent / conc. HCl / methanol

7: 84 percent / diisopropylethylamine / 0 °C

With hydrogenchloride; dmap; potassium hydroxide; sodium hydroxide; oxalyl dichloride; hydrazine hydrate; dimethyl sulfoxide; (+)-10-camphorsulfonic acid; triethylamine; N-ethyl-N,N-diisopropylamine; In methanol; ethanol; benzene;

Reference yield:

: 128466-21-7,128466-22-8
C₃₁H₃₃NO₅

: 128466-30-8
(1R,5S,9R)-3-Benzyl-1-methoxymethoxymethyl-5-methyl-3-aza-bicyclo[3.3.1]nonan-9-ol

Guidance literature:: Multi-step reaction with 8 steps

1: 100 percent / KOH / ethanol

2: (+)-10-camphorsulfonic acid / benzene / Heating

3: Et₃N, DMAP

4: 97 percent / KOH / ethanol

5: DMSO, (COCl)2, Et₃N

6: 68 percent / NH₂NH₂*H₂O, NaOH / various solvent(s)

7: 92 percent / conc. HCl / methanol

8: 84 percent / diisopropylethylamine / 0 °C

With hydrogenchloride; dmap; potassium hydroxide; sodium hydroxide; oxalyl dichloride; hydrazine hydrate; dimethyl sulfoxide; (+)-10-camphorsulfonic acid; triethylamine; N-ethyl-N,N-diisopropylamine; In methanol; ethanol; benzene;