(1R,5S,9S)-3-Benzyl-1,5-bis-hydroxymethyl-3-aza-bicyclo[3.3.1]nonan-9-ol

Base Information

Chemical Name:(1R,5S,9S)-3-Benzyl-1,5-bis-hydroxymethyl-3-aza-bicyclo[3.3.1]nonan-9-ol
CAS No.:128466-23-9
Molecular Formula:C₁₇H₂₅NO₃
Molecular Weight:291.39
Hs Code.:

Synonyms:(1R,5S,9S)-3-Benzyl-1,5-bis-hydroxymethyl-3-aza-bicyclo[3.3.1]nonan-9-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,5S,9S)-3-Benzyl-1,5-bis-hydroxymethyl-3-aza-bicyclo[3.3.1]nonan-9-ol

Chemical Property:

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Technology Process of (1R,5S,9S)-3-Benzyl-1,5-bis-hydroxymethyl-3-aza-bicyclo[3.3.1]nonan-9-ol

There total 1 articles about (1R,5S,9S)-3-Benzyl-1,5-bis-hydroxymethyl-3-aza-bicyclo[3.3.1]nonan-9-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 128466-21-7,128466-22-8
C₃₁H₃₃NO₅

: 128466-23-9
(1R,5S,9S)-3-Benzyl-1,5-bis-hydroxymethyl-3-aza-bicyclo[3.3.1]nonan-9-ol

Guidance literature:: With potassium hydroxide; In ethanol;

Reference yield:

: 128466-23-9
(1R,5S,9S)-3-Benzyl-1,5-bis-hydroxymethyl-3-aza-bicyclo[3.3.1]nonan-9-ol

: 128466-29-5
(1R,5S,9R)-3-Benzyl-1-hydroxymethyl-5-methyl-3-aza-bicyclo[3.3.1]nonan-9-ol

Guidance literature:: Multi-step reaction with 6 steps

1: (+)-10-camphorsulfonic acid / benzene / Heating

2: Et₃N, DMAP

3: 97 percent / KOH / ethanol

4: DMSO, (COCl)2, Et₃N

5: 68 percent / NH₂NH₂*H₂O, NaOH / various solvent(s)

6: 92 percent / conc. HCl / methanol

With hydrogenchloride; dmap; potassium hydroxide; sodium hydroxide; oxalyl dichloride; hydrazine hydrate; dimethyl sulfoxide; (+)-10-camphorsulfonic acid; triethylamine; In methanol; ethanol; benzene;

Reference yield:

: 128466-23-9
(1R,5S,9S)-3-Benzyl-1,5-bis-hydroxymethyl-3-aza-bicyclo[3.3.1]nonan-9-ol

: 128466-30-8
(1R,5S,9R)-3-Benzyl-1-methoxymethoxymethyl-5-methyl-3-aza-bicyclo[3.3.1]nonan-9-ol

Guidance literature:: Multi-step reaction with 7 steps

1: (+)-10-camphorsulfonic acid / benzene / Heating

2: Et₃N, DMAP

3: 97 percent / KOH / ethanol

4: DMSO, (COCl)2, Et₃N

5: 68 percent / NH₂NH₂*H₂O, NaOH / various solvent(s)

6: 92 percent / conc. HCl / methanol

7: 84 percent / diisopropylethylamine / 0 °C

With hydrogenchloride; dmap; potassium hydroxide; sodium hydroxide; oxalyl dichloride; hydrazine hydrate; dimethyl sulfoxide; (+)-10-camphorsulfonic acid; triethylamine; N-ethyl-N,N-diisopropylamine; In methanol; ethanol; benzene;