C₃₃H₂₉N₅O₃

Base Information

Chemical Name:C₃₃H₂₉N₅O₃
CAS No.:1431639-70-1
Molecular Formula:C₃₃H₂₉N₅O₃
Molecular Weight:543.625
Hs Code.:

C<sub>33</sub>H<sub>29</sub>N<sub>5</sub>O<sub>3</sub>

Synonyms:C₃₃H₂₉N₅O₃

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Chemical Property of C₃₃H₂₉N₅O₃

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Technology Process of C₃₃H₂₉N₅O₃

There total 7 articles about C₃₃H₂₉N₅O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1431639-68-7
5,5'-(4-methoxyphenylazanediyl)dipicolinaldehyde

: 104-94-9
4-methoxy-aniline

: 1431639-70-1
C₃₃H₂₉N₅O₃

Guidance literature:: With magnesium sulfate; In dichloromethane; for 48h;
DOI:10.1016/j.poly.2012.06.059

Reference yield:

: 624-28-2
2,5-dibromopyridine

: 1431639-70-1
C₃₃H₂₉N₅O₃

Guidance literature:: Multi-step reaction with 6 steps

1: n-butyllithium / toluene / 6 h / -78 - -10 °C

2: toluene-4-sulfonic acid / 48 h / Reflux

3: N,N`-dimethylethylenediamine; copper(l) iodide; sodium iodide / 1,4-dioxane / 72 h / Reflux

4: palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; caesium carbonate / toluene / 72 h / 95 °C / Inert atmosphere; Schlenk technique

5: hydrogenchloride / tetrahydrofuran / 48 h

6: magnesium sulfate / dichloromethane / 48 h

With hydrogenchloride; copper(l) iodide; n-butyllithium; palladium diacetate; magnesium sulfate; caesium carbonate; toluene-4-sulfonic acid; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium iodide; N,N`-dimethylethylenediamine; In tetrahydrofuran; 1,4-dioxane; dichloromethane; toluene;
DOI:10.1016/j.poly.2012.06.059

Reference yield:

: 31181-90-5
5-bromo-pyridine-2-carbaldehyde

: 1431639-70-1
C₃₃H₂₉N₅O₃

Guidance literature:: Multi-step reaction with 5 steps

1: toluene-4-sulfonic acid / 48 h / Reflux

2: N,N`-dimethylethylenediamine; copper(l) iodide; sodium iodide / 1,4-dioxane / 72 h / Reflux

3: palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; caesium carbonate / toluene / 72 h / 95 °C / Inert atmosphere; Schlenk technique

4: hydrogenchloride / tetrahydrofuran / 48 h

5: magnesium sulfate / dichloromethane / 48 h

With hydrogenchloride; copper(l) iodide; palladium diacetate; magnesium sulfate; caesium carbonate; toluene-4-sulfonic acid; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium iodide; N,N`-dimethylethylenediamine; In tetrahydrofuran; 1,4-dioxane; dichloromethane; toluene;
DOI:10.1016/j.poly.2012.06.059