Technology Process of C32H34N6O7S
There total 8 articles about C32H34N6O7S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 5 h / 20 °C / Cooling with ice
2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.33 h / 20 °C
2.2: 16 h / 100 °C / Inert atmosphere
With
sodium hydride; 3-chloro-benzenecarboperoxoic acid;
In
dichloromethane; N,N-dimethyl-formamide; mineral oil;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydrogencarbonate; tert-butyl alcohol / 40 h / Reflux
2.1: dimethyl sulfoxide / 16 h / 100 °C
3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 5 h / 20 °C / Cooling with ice
4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.33 h / 20 °C
4.2: 16 h / 100 °C / Inert atmosphere
With
sodium hydride; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; tert-butyl alcohol;
In
dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; mineral oil;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: dimethyl sulfoxide / 16 h / 100 °C
2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 5 h / 20 °C / Cooling with ice
3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.33 h / 20 °C
3.2: 16 h / 100 °C / Inert atmosphere
With
sodium hydride; 3-chloro-benzenecarboperoxoic acid;
In
dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; mineral oil;