2-(2-aminoethoxy)ethyl 4-(N-(2-(naphthalen-2-yl)imidazo[1,2-a]pyrazin-8-yl)sulfamoyl)phenylcarbamate

Base Information

Chemical Name:2-(2-aminoethoxy)ethyl 4-(N-(2-(naphthalen-2-yl)imidazo[1,2-a]pyrazin-8-yl)sulfamoyl)phenylcarbamate
CAS No.:1415830-70-4
Molecular Formula:C₂₇H₂₆N₆O₅S
Molecular Weight:546.607
Hs Code.:

Synonyms:2-(2-aminoethoxy)ethyl 4-(N-(2-(naphthalen-2-yl)imidazo[1,2-a]pyrazin-8-yl)sulfamoyl)phenylcarbamate

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Chemical Property of 2-(2-aminoethoxy)ethyl 4-(N-(2-(naphthalen-2-yl)imidazo[1,2-a]pyrazin-8-yl)sulfamoyl)phenylcarbamate

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Technology Process of 2-(2-aminoethoxy)ethyl 4-(N-(2-(naphthalen-2-yl)imidazo[1,2-a]pyrazin-8-yl)sulfamoyl)phenylcarbamate

There total 8 articles about 2-(2-aminoethoxy)ethyl 4-(N-(2-(naphthalen-2-yl)imidazo[1,2-a]pyrazin-8-yl)sulfamoyl)phenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1415830-69-1
C₃₂H₃₄N₆O₇S

: 1415830-70-4
2-(2-aminoethoxy)ethyl 4-(N-(2-(naphthalen-2-yl)imidazo[1,2-a]pyrazin-8-yl)sulfamoyl)phenylcarbamate

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 3h; Cooling with ice;

Reference yield:

: 138-41-0
4-(aminosulfonyl)-benzoic acid

: 1415830-70-4
2-(2-aminoethoxy)ethyl 4-(N-(2-(naphthalen-2-yl)imidazo[1,2-a]pyrazin-8-yl)sulfamoyl)phenylcarbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium azide; triphenylphosphine; trichloroacetonitrile / acetone / 18 h / 20 °C

2.1: toluene / 16 h / Reflux

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.33 h / 20 °C

3.2: 16 h / 100 °C / Inert atmosphere

4.1: trifluoroacetic acid / dichloromethane / 3 h / 20 °C / Cooling with ice

With sodium azide; sodium hydride; trichloroacetonitrile; triphenylphosphine; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide; acetone; toluene; mineral oil;

Reference yield:

: 1415830-52-2
8-(methylthio)-2-(naphthalen-2-yl)imidazo[1,2-a]pyrazine

: 1415830-70-4
2-(2-aminoethoxy)ethyl 4-(N-(2-(naphthalen-2-yl)imidazo[1,2-a]pyrazin-8-yl)sulfamoyl)phenylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 5 h / 20 °C / Cooling with ice

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.33 h / 20 °C

2.2: 16 h / 100 °C / Inert atmosphere

3.1: trifluoroacetic acid / dichloromethane / 3 h / 20 °C / Cooling with ice

With sodium hydride; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide; mineral oil;