Technology Process of C25H27N3O4
There total 5 articles about C25H27N3O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium hydrogencarbonate; Dess-Martin periodane;
In
dichloromethane;
at 20 ℃;
for 5h;
DOI:10.1021/acs.jmedchem.0c02258
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: hydrogenchloride / dichloromethane / 12 h / 20 °C
2.1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / dichloromethane / 0.5 h / -20 °C
2.2: 12 h / -20 °C
3.1: sodium tetrahydroborate / 3 h / 0 - 20 °C
4.1: Dess-Martin periodane; sodium hydrogencarbonate / dichloromethane / 5 h / 20 °C
With
hydrogenchloride; sodium tetrahydroborate; sodium hydrogencarbonate; Dess-Martin periodane; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate;
In
dichloromethane;
DOI:10.1021/acs.jmedchem.0c02258
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium tetrahydroborate / 3 h / 0 - 20 °C
2: Dess-Martin periodane; sodium hydrogencarbonate / dichloromethane / 5 h / 20 °C
With
sodium tetrahydroborate; sodium hydrogencarbonate; Dess-Martin periodane;
In
dichloromethane;
DOI:10.1021/acs.jmedchem.0c02258