(2'S,3'S)-methyl 2-[3-(benzyloxycarbonylamino)-2-hydroxy-4,4-dimethylpentyl]propenoate

Base Information

Chemical Name:(2'S,3'S)-methyl 2-[3-(benzyloxycarbonylamino)-2-hydroxy-4,4-dimethylpentyl]propenoate
CAS No.:241149-84-8
Molecular Formula:C₁₉H₂₇NO₅
Molecular Weight:349.427
Hs Code.:

Synonyms:(2'S,3'S)-methyl 2-[3-(benzyloxycarbonylamino)-2-hydroxy-4,4-dimethylpentyl]propenoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2'S,3'S)-methyl 2-[3-(benzyloxycarbonylamino)-2-hydroxy-4,4-dimethylpentyl]propenoate

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Technology Process of (2'S,3'S)-methyl 2-[3-(benzyloxycarbonylamino)-2-hydroxy-4,4-dimethylpentyl]propenoate

There total 2 articles about (2'S,3'S)-methyl 2-[3-(benzyloxycarbonylamino)-2-hydroxy-4,4-dimethylpentyl]propenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 4224-69-5
methyl 2-(bromomethyl)propenoate

: 143915-13-3
Z-Tle-H

: (2'R,3'S)-methyl 2-[3-(benzyloxycarbonylamino)-2-hydroxy-4,4-dimethylpentyl]propenoate

: 241149-84-8
(2'S,3'S)-methyl 2-[3-(benzyloxycarbonylamino)-2-hydroxy-4,4-dimethylpentyl]propenoate

Guidance literature:: With indium; water; In ethanol; at 20 ℃; for 4h;
DOI:10.1002/(sici)1099-0690(199907)1999:7<1551::aid-ejoc1551>3.0.co;2-8

Reference yield:

: 848777-16-2,186692-52-4
benzyl N-[(1S)-1-(hydroxymethyl)-2,2-dimethyl-propyl]carbamate

: 241149-84-8
(2'S,3'S)-methyl 2-[3-(benzyloxycarbonylamino)-2-hydroxy-4,4-dimethylpentyl]propenoate

Guidance literature:: Multi-step reaction with 2 steps

1: Dess-Martin periodinane / CH₂Cl₂ / 20 °C

2: 88 percent / indium; water / ethanol / 4 h / 20 °C

With indium; water; Dess-Martin periodane; In ethanol; dichloromethane; 1: Oxidation / 2: Addition;
DOI:10.1002/(sici)1099-0690(199907)1999:7<1551::aid-ejoc1551>3.0.co;2-8