tert-butyl (R)-(1-((3-hydroxypropyl)diphenylsilyl)-3-methylbutyl)carbamate

Base Information

Chemical Name:tert-butyl (R)-(1-((3-hydroxypropyl)diphenylsilyl)-3-methylbutyl)carbamate
CAS No.:1227297-05-3
Molecular Formula:C₂₅H₃₇NO₃Si
Molecular Weight:427.659
Hs Code.:

Synonyms:tert-butyl (R)-(1-((3-hydroxypropyl)diphenylsilyl)-3-methylbutyl)carbamate

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Chemical Property of tert-butyl (R)-(1-((3-hydroxypropyl)diphenylsilyl)-3-methylbutyl)carbamate

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Technology Process of tert-butyl (R)-(1-((3-hydroxypropyl)diphenylsilyl)-3-methylbutyl)carbamate

There total 5 articles about tert-butyl (R)-(1-((3-hydroxypropyl)diphenylsilyl)-3-methylbutyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: C₂₀H₂₉NOSi*ClH

: 1227297-05-3
tert-butyl (R)-(1-((3-hydroxypropyl)diphenylsilyl)-3-methylbutyl)carbamate

Guidance literature:: di-tert-butyl dicarbonate; C₂₀H₂₉NOSi*ClH; With triethylamine; In dichloromethane; at 20 ℃; for 18h; Inert atmosphere;

With water; sodium hydroxide; In dichloromethane; for 2h; Inert atmosphere;
DOI:10.1021/jo100301n

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: C₂₀H₂₉NOSi

: 1227297-05-3
tert-butyl (R)-(1-((3-hydroxypropyl)diphenylsilyl)-3-methylbutyl)carbamate

Guidance literature:: With triethylamine;
DOI:10.1021/ol101379t

Reference yield:

: 775-12-2
diphenylsilane

: 1227297-05-3
tert-butyl (R)-(1-((3-hydroxypropyl)diphenylsilyl)-3-methylbutyl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: Wilkinson's catalyst / tetrahydrofuran / Inert atmosphere

2.1: lithium / tetrahydrofuran / Inert atmosphere

2.2: Inert atmosphere

3.1: hydrogenchloride / methanol / Inert atmosphere

3.2: Inert atmosphere

3.3: Inert atmosphere

With hydrogenchloride; Wilkinson's catalyst; lithium; In tetrahydrofuran; methanol;
DOI:10.1021/jm301000k