(2-{4-[4-(4-chlorophenyl)-5-oxo-2,5-dihydrofuran-3-yl]benzenesulfonylamino}ethyl)carbamic acid tert-butyl ester

Base Information

Chemical Name:(2-{4-[4-(4-chlorophenyl)-5-oxo-2,5-dihydrofuran-3-yl]benzenesulfonylamino}ethyl)carbamic acid tert-butyl ester
CAS No.:1416368-37-0
Molecular Formula:C₂₃H₂₅ClN₂O₆S
Molecular Weight:492.98
Hs Code.:

Synonyms:(2-{4-[4-(4-chlorophenyl)-5-oxo-2,5-dihydrofuran-3-yl]benzenesulfonylamino}ethyl)carbamic acid tert-butyl ester

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Chemical Property of (2-{4-[4-(4-chlorophenyl)-5-oxo-2,5-dihydrofuran-3-yl]benzenesulfonylamino}ethyl)carbamic acid tert-butyl ester

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Technology Process of (2-{4-[4-(4-chlorophenyl)-5-oxo-2,5-dihydrofuran-3-yl]benzenesulfonylamino}ethyl)carbamic acid tert-butyl ester

There total 1 articles about (2-{4-[4-(4-chlorophenyl)-5-oxo-2,5-dihydrofuran-3-yl]benzenesulfonylamino}ethyl)carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 57260-73-8
N-BOC-1,2-diaminoethane

: 1044169-18-7
4-[4-(4-chloro-phenyl)-5-oxo-2,5-dihydro-furan-3-yl]-benzenesulfonyl chloride

: 1416368-37-0
(2-{4-[4-(4-chlorophenyl)-5-oxo-2,5-dihydrofuran-3-yl]benzenesulfonylamino}ethyl)carbamic acid tert-butyl ester

Guidance literature:: With triethylamine; In tetrahydrofuran; at 25 ℃; for 6h; Inert atmosphere;
DOI:10.1016/j.bmcl.2012.10.131

Reference yield:

: 1416368-37-0
(2-{4-[4-(4-chlorophenyl)-5-oxo-2,5-dihydrofuran-3-yl]benzenesulfonylamino}ethyl)carbamic acid tert-butyl ester

: C₁₈H₁₇ClN₂O₄S

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 25 ℃; for 6h;
DOI:10.1016/j.bmcl.2012.10.131

Reference yield:

: 1416368-37-0
(2-{4-[4-(4-chlorophenyl)-5-oxo-2,5-dihydrofuran-3-yl]benzenesulfonylamino}ethyl)carbamic acid tert-butyl ester

: 1416368-38-1
C₃₀H₂₈ClN₃O₆S₂

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 6 h / 25 °C

2: triethylamine / dichloromethane / 5 h / 25 °C / Inert atmosphere

With triethylamine; trifluoroacetic acid; In dichloromethane;
DOI:10.1016/j.bmcl.2012.10.131