3α-acetyloxy-12α-hydroxy-5β-cholan-24-oic acid

Base Information

Chemical Name:3α-acetyloxy-12α-hydroxy-5β-cholan-24-oic acid
CAS No.:63060-59-3
Molecular Formula:C₂₆H₄₂O₅
Molecular Weight:434.616
Hs Code.:

Synonyms:3α-acetyloxy-12α-hydroxy-5β-cholan-24-oic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3α-acetyloxy-12α-hydroxy-5β-cholan-24-oic acid

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Technology Process of 3α-acetyloxy-12α-hydroxy-5β-cholan-24-oic acid

There total 1 articles about 3α-acetyloxy-12α-hydroxy-5β-cholan-24-oic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 57-88-5
cholesterol

: 83-44-3
Deoxycholic acid

: 108-24-7
acetic anhydride

: 604-35-3
Cholesteryl acetate

: 63060-59-3
3α-acetyloxy-12α-hydroxy-5β-cholan-24-oic acid

Guidance literature:: With C₅₀H₇₆N₁₈O₁₆; triethylamine; In chloroform; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1002/chem.201600790

Reference yield: 78.0%

: 63060-59-3
3α-acetyloxy-12α-hydroxy-5β-cholan-24-oic acid

: 15028-39-4,13226-98-7
L-2-phenylglycine methyl ester hydrochloride

: 2-(3α-acetyloxy-12α-hydroxy-5β-cholan-24-oxo-24-yl)aminophenylacetic acid methyl ester

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 - 20 ℃; for 5.08h;
DOI:10.1248/cpb.c16-00836

Reference yield: 68.0%

: 63060-59-3
3α-acetyloxy-12α-hydroxy-5β-cholan-24-oic acid

: 7524-50-7
methyl (2S)-2-amino-3-phenylpropanoate hydrochloride

: 2-(3α-acetyloxy-12α-hydroxy-5β-cholan-24-oxo-24-yl)aminophenylpropionic acid methyl ester

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 - 20 ℃; for 5.08h;
DOI:10.1248/cpb.c16-00836