3,9,17,23-tetratosyl-3,9,17,23,29,30-hexaaza-6,20-dioxatricyclo<23.3.1.1^11,15>triaconta-1(29),11(30),12,14,25,27-hexaene

Base Information

• Chemical Name: 3,9,17,23-tetratosyl-3,9,17,23,29,30-hexaaza-6,20-dioxatricyclo<23.3.1.1^11,15>triaconta-1(29),11(30),12,14,25,27-hexaene
• CAS No.: 125682-95-3
• Molecular Formula: C₅₀H₅₈N₆O₁₀S₄
• Molecular Weight: 1031.31

Synonyms:3,9,17,23-tetratosyl-3,9,17,23,29,30-hexaaza-6,20-dioxatricyclo<23.3.1.1^11,15>triaconta-1(29),11(30),12,14,25,27-hexaene

Chemical Property of 3,9,17,23-tetratosyl-3,9,17,23,29,30-hexaaza-6,20-dioxatricyclo<23.3.1.1^11,15>triaconta-1(29),11(30),12,14,25,27-hexaene

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Technology Process of 3,9,17,23-tetratosyl-3,9,17,23,29,30-hexaaza-6,20-dioxatricyclo<23.3.1.1^11,15>triaconta-1(29),11(30),12,14,25,27-hexaene

There total 5 articles about 3,9,17,23-tetratosyl-3,9,17,23,29,30-hexaaza-6,20-dioxatricyclo<23.3.1.1^11,15>triaconta-1(29),11(30),12,14,25,27-hexaene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

2,6-bis<(p-tosylamino)methyl>pyridine (112633-27-9) + 2,6-bis<-N-tosylamino>methyl>pyridine (125682-94-2) → 3,9,17,23-tetratosyl-3,9,17,23,29,30-hexaaza-6,20-dioxatricyclo<23.3.1.111,15>triaconta-1(29),11(30),12,14,25,27-hexaene (125682-95-3)

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; at 85 ℃; for 48h;

DOI:10.1002/hlca.19890720525

Reference yield:

2,6-bis(aminomethyl)pyridine (34984-16-2) → 3,9,17,23-tetratosyl-3,9,17,23,29,30-hexaaza-6,20-dioxatricyclo<23.3.1.111,15>triaconta-1(29),11(30),12,14,25,27-hexaene (125682-95-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 94 percent

2: 32 percent / Cs₂CO₃ / dimethylformamide / 48 h / 85 °C

With caesium carbonate; In N,N-dimethyl-formamide;

DOI:10.1002/hlca.19890720525

Reference yield:

p-toluenesulfonyl chloride (98-59-9) → 3,9,17,23-tetratosyl-3,9,17,23,29,30-hexaaza-6,20-dioxatricyclo<23.3.1.111,15>triaconta-1(29),11(30),12,14,25,27-hexaene (125682-95-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 94 percent

2: 32 percent / Cs₂CO₃ / dimethylformamide / 48 h / 85 °C

With caesium carbonate; In N,N-dimethyl-formamide;

DOI:10.1002/hlca.19890720525

upstream raw materials:

2,6-bis<(p-tosylamino)methyl>pyridine

2,6-bis<-N-tosylamino>methyl>pyridine

2,6-bis(aminomethyl)pyridine

p-toluenesulfonyl chloride

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