2,6-PyridinediMethanaMine

Base Information

• Chemical Name: 2,6-PyridinediMethanaMine
• CAS No.: 34984-16-2
• Molecular Formula: C₇H₁₁N₃
• Molecular Weight: 137.184
• Hs Code.: 2933399990
• Mol file: 34984-16-2.mol

Synonyms:2,6-bis(aminomethyl)pyridine

Chemical Property of 2,6-PyridinediMethanaMine

Chemical Property:

• Boiling Point: 257.5±30.0 °C(Predicted)
• PKA: 8.99±0.39(Predicted)
• Density: 1.118±0.06 g/cm3(Predicted)
• Sensitive.: air sensitive

Purity/Quality:

≥99% ^*data from raw suppliers

2,6-Bis(aminomethyl)pyridine, min. 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,6-PyridinediMethanaMine

There total 15 articles about 2,6-PyridinediMethanaMine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

2,6-bis(azidomethyl)pyridine (200489-04-9) → 2,6-bis(aminomethyl)pyridine (34984-16-2)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In ethanol; at 20 ℃; for 3h; Inert atmosphere;

DOI:10.1021/acs.organomet.1c00100

Reference yield: 85.0%

2,6-bis(phthalimidomethyl)pyridine (67455-81-6) → 2,6-bis(aminomethyl)pyridine (34984-16-2)

Guidance literature:

With hydrazine hydrate; In ethanol; Inert atmosphere; Reflux;

DOI:10.1039/c7ob02508d

Reference yield: 75.0%

2,6-bis-(bromomethyl)pyridine (7703-74-4) → 2,6-bis(aminomethyl)pyridine (34984-16-2)

Guidance literature:

2,6-bis-(bromomethyl)pyridine; With potassium phtalimide; In N,N-dimethyl-formamide; at 100 ℃; for 48h;

With hydrazine hydrate; In ethanol; water; at 20 ℃; for 24h; Reflux;

With hydrogenchloride; In ethanol; water; at 20 ℃; for 12h; Reflux;

DOI:10.1039/c6cc09206c

upstream raw materials:

pyridine-2,6-dinitrile

pyridine-2,6-dicarbaldehyde dioxime

pyridine-2,6-dicarboxylic acid diamide

2.6-bis(hydroxymethyl)pyridine

Downstream raw materials:

2,2'-(pyridine-2,6-diyldimethyldiimino-dimethyl)-bis-phenol

2,6-Bis(3,4,5-trimethoxybenzoylaminomethyl)pyridine

2,6-bis<(p-tosylamino)methyl>pyridine

2,6-bis-(benzoylamino-methyl)-pyridine