C₁₆H₁₅ClN₂O₄

Base Information

Chemical Name:C₁₆H₁₅ClN₂O₄
CAS No.:1426320-74-2
Molecular Formula:C₁₆H₁₅ClN₂O₄
Molecular Weight:334.759
Hs Code.:

C<sub>16</sub>H<sub>15</sub>ClN<sub>2</sub>O<sub>4</sub>

Synonyms:C₁₆H₁₅ClN₂O₄

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Chemical Property of C₁₆H₁₅ClN₂O₄

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Technology Process of C₁₆H₁₅ClN₂O₄

There total 6 articles about C₁₆H₁₅ClN₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 453-20-3,84921-89-1,864447-89-2
3-Hydroxytetrahydrofuran

: 1426320-73-1
C₁₂H₉ClN₂O₃

: 1426320-74-2
C₁₆H₁₅ClN₂O₄

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

Reference yield:

: 1426320-72-0
C₁₁H₇ClN₂O₃

: 1426320-74-2
C₁₆H₁₅ClN₂O₄

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid / 4 h / Reflux

2: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

With di-isopropyl azodicarboxylate; sulfuric acid; triphenylphosphine; In tetrahydrofuran;

Reference yield:

: 16817-43-9
5-Bromo-2-chloroanisole

: 1426320-74-2
C₁₆H₁₅ClN₂O₄

Guidance literature:: Multi-step reaction with 6 steps

1.1: n-butyllithium / tetrahydrofuran; toluene / 0.5 h / -78 °C / Inert atmosphere

1.2: 16 h / 20 °C

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,4-dioxane / 3 h / 90 °C / Inert atmosphere

3.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; triethylamine / 16 h / 50 °C / 3750.38 Torr / Inert atmosphere

4.1: boron tribromide / dichloromethane / -78 - 20 °C / Inert atmosphere

5.1: sulfuric acid / 4 h / Reflux

6.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; di-isopropyl azodicarboxylate; sulfuric acid; boron tribromide; potassium carbonate; triethylamine; triphenylphosphine; In tetrahydrofuran; 1,4-dioxane; dichloromethane; toluene;