(6-chloro-2,4-diphenylquinolin-3-yl)diphenylphosphine oxide

Base Information

• Chemical Name: (6-chloro-2,4-diphenylquinolin-3-yl)diphenylphosphine oxide
• CAS No.: 1260254-89-4
• Molecular Formula: C₃₃H₂₃ClNOP
• Molecular Weight: 515.978
• Mol file: 1260254-89-4.mol

Synonyms:(6-chloro-2,4-diphenylquinolin-3-yl)diphenylphosphine oxide

Chemical Property of (6-chloro-2,4-diphenylquinolin-3-yl)diphenylphosphine oxide

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of (6-chloro-2,4-diphenylquinolin-3-yl)diphenylphosphine oxide

There total 2 articles about (6-chloro-2,4-diphenylquinolin-3-yl)diphenylphosphine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

phenacyldiphenylphosphine oxide (1733-58-0) + 5-chloro-2-aminobenzophenone (719-59-5) → (6-chloro-2,4-diphenylquinolin-3-yl)diphenylphosphine oxide (1260254-89-4)

Guidance literature:

With toluene-4-sulfonic acid; In toluene; for 36h; Reflux;

DOI:10.1080/10426501003671429

Reference yield: 76.0%

Diphenylphosphine oxide (4559-70-0) + N-(1-phenyl-3-phenyl-2-propynyl)-4-chloroaniline → (6-chloro-2,4-diphenylquinolin-3-yl)diphenylphosphine oxide (1260254-89-4)

Guidance literature:

With [bis(acetoxy)iodo]benzene; fac-tris[2-phenylpyridinato-C²,N]iridium(III); sodium hydrogencarbonate; In N,N-dimethyl-formamide; at 20 ℃; for 36h; Inert atmosphere; Schlenk technique; Irradiation;

DOI:10.1039/c7cc02433a

upstream raw materials:

phenacyldiphenylphosphine oxide

5-chloro-2-aminobenzophenone

Diphenylphosphine oxide