C₆₀H₃₈B₂N₆O₂

Base Information

Chemical Name:C₆₀H₃₈B₂N₆O₂
CAS No.:1392132-15-8
Molecular Formula:C₆₀H₃₈B₂N₆O₂
Molecular Weight:896.623
Hs Code.:

C<sub>60</sub>H<sub>38</sub>B<sub>2</sub>N<sub>6</sub>O<sub>2</sub>

Synonyms:C₆₀H₃₈B₂N₆O₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₆₀H₃₈B₂N₆O₂

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Technology Process of C₆₀H₃₈B₂N₆O₂

There total 9 articles about C₆₀H₃₈B₂N₆O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1392132-14-7
methoxy(5,10-diphenyl-15-trimethylsilylethynylsubporphyrinato)boron(III)

: 1392132-15-8
C₆₀H₃₈B₂N₆O₂

Guidance literature:: With tetrabutylammonium fluoride; Cu(CH₃COO)2; In tetrahydrofuran; pyridine; deprotection with tetrabutylammonium fluoride in THF/CH3OH; dimerizationby treatment with Cu(CH3COO)2 in pyridine/THF;
DOI:10.1002/anie.201201853

Reference yield:

: 195381-16-9
5,10-diphenyltripyrrane

: 1392132-15-8
C₆₀H₃₈B₂N₆O₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: 1,2-dichloro-benzene / 2 h / 150 °C / Inert atmosphere

2.1: 1,2-dichloro-benzene / 1 h / 100 °C

2.2: air / 1 h / Reflux

3.1: N-Bromosuccinimide / chloroform / 0.25 h / 0 °C

4.1: copper(l) iodide; bis(triphenylphosphine)palladium(II) chloride; diisopropylamine / toluene / 12 h / 80 °C / Inert atmosphere

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran; methanol / 1 h / Inert atmosphere

6.1: copper diacetate / tetrahydrofuran; pyridine / 1 h / Inert atmosphere

With N-Bromosuccinimide; copper(l) iodide; bis(triphenylphosphine)palladium(II) chloride; tetrabutyl ammonium fluoride; copper diacetate; diisopropylamine; In tetrahydrofuran; pyridine; methanol; chloroform; 1,2-dichloro-benzene; toluene; 4.1: Sonogashira coupling;
DOI:10.1002/anie.201201853

Reference yield:

: 1392132-03-4
methoxo(5,10-diphenylsubporphyrinato)boron(III)

: 1392132-15-8
C₆₀H₃₈B₂N₆O₂

Guidance literature:: Multi-step reaction with 4 steps

1: N-Bromosuccinimide / chloroform / 0.25 h / 0 °C

2: copper(l) iodide; bis(triphenylphosphine)palladium(II) chloride; diisopropylamine / toluene / 12 h / 80 °C / Inert atmosphere

3: tetrabutyl ammonium fluoride / tetrahydrofuran; methanol / 1 h / Inert atmosphere

4: copper diacetate / tetrahydrofuran; pyridine / 1 h / Inert atmosphere

With N-Bromosuccinimide; copper(l) iodide; bis(triphenylphosphine)palladium(II) chloride; tetrabutyl ammonium fluoride; copper diacetate; diisopropylamine; In tetrahydrofuran; pyridine; methanol; chloroform; toluene; 2: Sonogashira coupling;
DOI:10.1002/anie.201201853