methyl N-[pyrrolidin-2-ylcarbonyl]-O-{2-[6-(methylamino)pyridin-2-yl]ethyl}-L-tyrosinate

Base Information

• Chemical Name: methyl N-[pyrrolidin-2-ylcarbonyl]-O-{2-[6-(methylamino)pyridin-2-yl]ethyl}-L-tyrosinate
• CAS No.: 1041664-20-3
• Molecular Formula: C₂₃H₃₀N₄O₄
• Molecular Weight: 426.516

Synonyms:methyl N-[pyrrolidin-2-ylcarbonyl]-O-{2-[6-(methylamino)pyridin-2-yl]ethyl}-L-tyrosinate

Chemical Property of methyl N-[pyrrolidin-2-ylcarbonyl]-O-{2-[6-(methylamino)pyridin-2-yl]ethyl}-L-tyrosinate

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Technology Process of methyl N-[pyrrolidin-2-ylcarbonyl]-O-{2-[6-(methylamino)pyridin-2-yl]ethyl}-L-tyrosinate

There total 1 articles about methyl N-[pyrrolidin-2-ylcarbonyl]-O-{2-[6-(methylamino)pyridin-2-yl]ethyl}-L-tyrosinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

methyl N-[(1-(tert-butoxycarbonyl)pyrrolidin-2-yl)carbonyl]-O-{2-[6-(methylamino)pyridin-2-yl]ethyl}-L-tyrosinate (1041664-17-8) → methyl N-[pyrrolidin-2-ylcarbonyl]-O-{2-[6-(methylamino)pyridin-2-yl]ethyl}-L-tyrosinate (1041664-20-3)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 17 - 25 ℃; for 16h;

Reference yield: 61.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + methyl N-[pyrrolidin-2-ylcarbonyl]-O-{2-[6-(methylamino)pyridin-2-yl]ethyl}-L-tyrosinate (1041664-20-3) → methyl N-[(1-methylpyrrolidin-2-yl)carbonyl]-O-{2-[6-(methylamino)pyridin-2-yl]ethyl}-L-tyrosinate (1041664-11-2)

Guidance literature:

With sodium tris(acetoxy)borohydride; acetic acid; In methanol; dichloromethane; at 17 - 25 ℃; for 4h;

Reference yield: 53.0%

methyl N-[pyrrolidin-2-ylcarbonyl]-O-{2-[6-(methylamino)pyridin-2-yl]ethyl}-L-tyrosinate (1041664-20-3) + acetone (67-64-1) → methyl N-[(1-isopropylpyrrolidin-2-yl)carbonyl]-O-{2-[6-(methylamino)pyridin-2-yl]ethyl}-L-tyrosinate (1041664-26-9)

Guidance literature:

With sodium tris(acetoxy)borohydride; acetic acid; In methanol; dichloromethane; at 17 - 25 ℃; for 3h;

upstream raw materials:

methyl N-[(1-(tert-butoxycarbonyl)pyrrolidin-2-yl)carbonyl]-O-{2-[6-(methylamino)pyridin-2-yl]ethyl}-L-tyrosinate

Downstream raw materials:

methyl N-[(1-methylpyrrolidin-2-yl)carbonyl]-O-{2-[6-(methylamino)pyridin-2-yl]ethyl}-L-tyrosinate

methyl N-[(1-isopropylpyrrolidin-2-yl)carbonyl]-O-{2-[6-(methylamino)pyridin-2-yl]ethyl}-L-tyrosinate

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