azidocobalt(III)tetraphenylporphyrin

Base Information

Chemical Name:azidocobalt(III)tetraphenylporphyrin
CAS No.:114055-75-3
Molecular Formula:C₄₄H₂₈CoN₇
Molecular Weight:713.746
Hs Code.:

Synonyms:azidocobalt(III)tetraphenylporphyrin

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Chemical Property of azidocobalt(III)tetraphenylporphyrin

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Technology Process of azidocobalt(III)tetraphenylporphyrin

There total 3 articles about azidocobalt(III)tetraphenylporphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: (tetraphenylporphyrinato)cobalt(III) tetrafluoroborate

: 114055-75-3
azidocobalt(III)tetraphenylporphyrin

Guidance literature:: With sodium azide; In dichloromethane; byproducts: NaBF4; stirring of (Co(TPP))BF4 and NaN3 in CH2Cl2 at room temp. for 18 h;; sepn. of NaBF4 by centrifugation; pptn. by addn. of n-pentane to the filtrate; centrifugation; washed three times with n-pentane; dried in a high-vac. for 5 h; elem. anal.;

Reference yield:

: 122070-43-3
N₃Co(III)TPP(py)

: 14172-90-8
cobalt(II) 5,10,15,20-tetraphenylporphyrin

: 114055-75-3
azidocobalt(III)tetraphenylporphyrin

Guidance literature:: In benzene; byproducts: N3, C6H5N; laser pulse, Ar-satd. soln.; optical absorption spectroscopy (quantum yield);
DOI:10.1021/j100355a017

Reference yield:

: sodium azide

: 60166-10-1
[5,10,15,20-tetraphenylporphyrin]cobalt(III) chloride

: 114055-75-3
azidocobalt(III)tetraphenylporphyrin

Guidance literature:: In methanol; dichloromethane; byproducts: Cl(1-); CH2Cl2 soln. of Co-compd. mixed with MeOH soln. of Na-compd., stirred vigorously for 3h, H2O added; extd. (CH2Cl2), evapd., chromy. (silica gel, CH2Cl2), recrystd. (CH2Cl2/hexane); elem. anal.;
DOI:10.1021/j100355a017