C₂₅H₂₇NO₆

Base Information

Chemical Name:C₂₅H₂₇NO₆
CAS No.:1246887-80-8
Molecular Formula:C₂₅H₂₇NO₆
Molecular Weight:437.492
Hs Code.:

C<sub>25</sub>H<sub>27</sub>NO<sub>6</sub>

Synonyms:C₂₅H₂₇NO₆

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Chemical Property of C₂₅H₂₇NO₆

Chemical Property:

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Technology Process of C₂₅H₂₇NO₆

There total 19 articles about C₂₅H₂₇NO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1246887-79-5
C₁₈H₂₄O₃

: 122-04-3
4-nitro-benzoyl chloride

: 1246887-80-8
C₂₅H₂₇NO₆

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/ja106585n

Reference yield:

: 1246887-72-8
C₂₁H₃₈O₂Si

: 1246887-80-8
C₂₅H₂₇NO₆

Guidance literature:: Multi-step reaction with 8 steps

1: 4-methylmorpholine N-oxide; tetrapropylammonium perruthennate / dichloromethane / Inert atmosphere; Molecular sieve

2: n-butyllithium / tetrahydrofuran / -78 °C / Inert atmosphere

3: phthalic acid dimethyl ester; sodium hydrogencarbonate / dichloromethane / Inert atmosphere

4: 2,6-di-tert-butyl-4-methyl-phenol / toluene / 24 h / Inert atmosphere; Reflux

5: tris(triphenylphosphine)rhodium(l) chloride; hydrogen / benzene / 3 h / 70 °C / Inert atmosphere

6: pyridine hydrogenfluoride / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

7: cerium(III) chloride heptahydrate; sodium tetrahydroborate / ethanol / 0.5 h / 0 °C / Inert atmosphere

8: triethylamine; dmap / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

With dmap; sodium tetrahydroborate; n-butyllithium; tetrapropylammonium perruthennate; tris(triphenylphosphine)rhodium(l) chloride; cerium(III) chloride heptahydrate; phthalic acid dimethyl ester; 2,6-di-tert-butyl-4-methyl-phenol; hydrogen; sodium hydrogencarbonate; pyridine hydrogenfluoride; 4-methylmorpholine N-oxide; triethylamine; In tetrahydrofuran; ethanol; dichloromethane; toluene; benzene;
DOI:10.1021/jo4006156

Reference yield:

: 139616-47-0
methyl (1S)-2-((1R,2R)-2-hydroxycycloheptan-1-yl)oxy-1-methyl-2-cyclopenten-1-carboxylate

: 1246887-80-8
C₂₅H₂₇NO₆

Guidance literature:: Multi-step reaction with 16 steps

1: triethylamine; iodine / tetrahydrofuran / 3 h / -40 °C / Inert atmosphere

2: 1,8-diazabicyclo[5.4.0]undec-7-ene / 3 h / 100 °C / Inert atmosphere

3: hydrogenchloride / methanol / 3 h / 20 °C / Inert atmosphere

4: tert.-butyl lithium / diethyl ether / -78 °C / Inert atmosphere

5: pyridinium chlorochromate / dichloromethane / Inert atmosphere

6: lithium triethylborohydride / tetrahydrofuran / Inert atmosphere

7: triethylamine / dichloromethane / Inert atmosphere

8: diisobutylaluminium hydride / dichloromethane / -78 °C / Inert atmosphere

9: 4-methylmorpholine N-oxide; tetrapropylammonium perruthennate / dichloromethane / Inert atmosphere; Molecular sieve

10: n-butyllithium / tetrahydrofuran / -78 °C / Inert atmosphere

11: phthalic acid dimethyl ester; sodium hydrogencarbonate / dichloromethane / Inert atmosphere

12: 2,6-di-tert-butyl-4-methyl-phenol / toluene / 24 h / Inert atmosphere; Reflux

13: tris(triphenylphosphine)rhodium(l) chloride; hydrogen / benzene / 3 h / 70 °C / Inert atmosphere

14: pyridine hydrogenfluoride / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

15: cerium(III) chloride heptahydrate; sodium tetrahydroborate / ethanol / 0.5 h / 0 °C / Inert atmosphere

16: triethylamine; dmap / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

With hydrogenchloride; dmap; sodium tetrahydroborate; n-butyllithium; tetrapropylammonium perruthennate; tris(triphenylphosphine)rhodium(l) chloride; cerium(III) chloride heptahydrate; phthalic acid dimethyl ester; 2,6-di-tert-butyl-4-methyl-phenol; hydrogen; iodine; tert.-butyl lithium; diisobutylaluminium hydride; lithium triethylborohydride; sodium hydrogencarbonate; pyridine hydrogenfluoride; 4-methylmorpholine N-oxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; pyridinium chlorochromate; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; toluene; benzene;
DOI:10.1021/jo4006156