methyl 2,4-dimethoxy-6-(7-methoxycarbonyl) heptyl benzoate

Base Information

Chemical Name:methyl 2,4-dimethoxy-6-(7-methoxycarbonyl) heptyl benzoate
CAS No.:130877-73-5
Molecular Formula:C₁₉H₂₈O₆
Molecular Weight:352.428
Hs Code.:

Synonyms:methyl 2,4-dimethoxy-6-(7-methoxycarbonyl) heptyl benzoate

Suppliers and Price of methyl 2,4-dimethoxy-6-(7-methoxycarbonyl) heptyl benzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2,4-dimethoxy-6-(7-methoxycarbonyl) heptyl benzoate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of methyl 2,4-dimethoxy-6-(7-methoxycarbonyl) heptyl benzoate

There total 11 articles about methyl 2,4-dimethoxy-6-(7-methoxycarbonyl) heptyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 130877-75-7
methyl 2,4-dimethoxy-6-<1-(p-tolylsulfonyl)-7-methoxycarbonyl heptyl> benzoate

: 130877-73-5
methyl 2,4-dimethoxy-6-(7-methoxycarbonyl) heptyl benzoate

Guidance literature:: With disodium hydrogenphosphate; sodium amalgam; In methanol; at -20 ℃; for 1h;
DOI:10.1016/0957-4166(90)90013-Z

Reference yield:

: 539-87-7
oxocan-2-one

: 130877-73-5
methyl 2,4-dimethoxy-6-(7-methoxycarbonyl) heptyl benzoate

Guidance literature:: Multi-step reaction with 5 steps

1: conc. H₂SO₄ / 2 h / Ambient temperature

2: 80 percent / Et₃N / CH₂Cl₂ / 2 h / Ambient temperature

3: NaI, NaHCO₃ / acetone / 72 h / Ambient temperature

4: 1.) LDA, 2.) HMPA / 1.) THF, -78 deg C, 1 h, 2.) 5 min

5: 98 percent / Na₂HPO₄, 6percent sodium amalgam / methanol / 1 h / -20 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; disodium hydrogenphosphate; sodium amalgam; sulfuric acid; sodium hydrogencarbonate; triethylamine; sodium iodide; lithium diisopropyl amide; In methanol; dichloromethane; acetone;
DOI:10.1016/0957-4166(90)90013-Z

Reference yield:

: 6110-37-8
methyl 2,4-dimethoxy-6-methylbenzoate

: 130877-73-5
methyl 2,4-dimethoxy-6-(7-methoxycarbonyl) heptyl benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) LDA / 1.) THF, -78 deg C, 15 min, 2.) 5 min

2: 94 percent / m-chloroperbenzoic acid (m-CPBA) / CH₂Cl₂ / 1 h / Ambient temperature

3: 1.) LDA, 2.) HMPA / 1.) THF, -78 deg C, 1 h, 2.) 5 min

4: 98 percent / Na₂HPO₄, 6percent sodium amalgam / methanol / 1 h / -20 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; disodium hydrogenphosphate; sodium amalgam; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In methanol; dichloromethane;
DOI:10.1016/0957-4166(90)90013-Z