3-(2-((tert-butyldiphenylsilyl)oxy)ethyl)-1-(pyrrolidin-1-yl)pent-4-en-1-one

Base Information

Chemical Name:3-(2-((tert-butyldiphenylsilyl)oxy)ethyl)-1-(pyrrolidin-1-yl)pent-4-en-1-one
CAS No.:1356570-93-8
Molecular Formula:C₂₇H₃₇NO₂Si
Molecular Weight:435.682
Hs Code.:

Synonyms:3-(2-((tert-butyldiphenylsilyl)oxy)ethyl)-1-(pyrrolidin-1-yl)pent-4-en-1-one

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Chemical Property of 3-(2-((tert-butyldiphenylsilyl)oxy)ethyl)-1-(pyrrolidin-1-yl)pent-4-en-1-one

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Technology Process of 3-(2-((tert-butyldiphenylsilyl)oxy)ethyl)-1-(pyrrolidin-1-yl)pent-4-en-1-one

There total 6 articles about 3-(2-((tert-butyldiphenylsilyl)oxy)ethyl)-1-(pyrrolidin-1-yl)pent-4-en-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1356570-91-6
3-(2-hydroxyethyl)-1-(pyrrolidin-1-yl)pent-4-en-1-one

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1356570-93-8
3-(2-((tert-butyldiphenylsilyl)oxy)ethyl)-1-(pyrrolidin-1-yl)pent-4-en-1-one

Guidance literature:: With 1H-imidazole; In dichloromethane; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1002/ejoc.201101343

Reference yield:

: 1356570-97-2
C₇H₁₁O₃^(1-)*Na⁽¹⁺⁾

: 1356570-93-8
3-(2-((tert-butyldiphenylsilyl)oxy)ethyl)-1-(pyrrolidin-1-yl)pent-4-en-1-one

Guidance literature:: Multi-step reaction with 5 steps

1: 1H-imidazole / tetrahydrofuran; N,N-dimethyl-formamide / 16 h / 20 °C / Inert atmosphere

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 24 h / 20 °C / Inert atmosphere

3: iodine / acetonitrile / 24 h / 0 °C / Inert atmosphere

4: benzene / Inert atmosphere; Heating

5: 1H-imidazole / dichloromethane / 16 h / 20 °C / Inert atmosphere

With 1H-imidazole; iodine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetonitrile; benzene;
DOI:10.1002/ejoc.201101343

Reference yield:

: 1356570-99-4
C₂₄H₃₂O₃Si

: 1356570-93-8
3-(2-((tert-butyldiphenylsilyl)oxy)ethyl)-1-(pyrrolidin-1-yl)pent-4-en-1-one

Guidance literature:: Multi-step reaction with 3 steps

1: iodine / acetonitrile / 24 h / 0 °C / Inert atmosphere

2: benzene / Inert atmosphere; Heating

3: 1H-imidazole / dichloromethane / 16 h / 20 °C / Inert atmosphere

With 1H-imidazole; iodine; In dichloromethane; acetonitrile; benzene;
DOI:10.1002/ejoc.201101343