Technology Process of C31H37N5O4
There total 6 articles about C31H37N5O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C26H37N3O6S;
With
lithium tert-butoxide; XPhos;
tris-(dibenzylideneacetone)dipalladium(0);
In
1,4-dioxane;
at 20 ℃;
Inert atmosphere;
7‐bromo‐2‐(1‐methyl‐1H‐pyrazol‐4‐yl)quinoxaline;
In
1,4-dioxane;
at 110 ℃;
for 12h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: trichlorophosphate / 2 h / 100 °C
2.1: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane; water / 15 h / Inert atmosphere; Reflux
3.1: lithium tert-butoxide; XPhos / tris-(dibenzylideneacetone)dipalladium(0) / 1,4-dioxane / 20 °C / Inert atmosphere
3.2: 12 h / 110 °C
With
sodium carbonate; lithium tert-butoxide; XPhos; trichlorophosphate;
tris-(dibenzylideneacetone)dipalladium(0); tetrakis(triphenylphosphine) palladium(0);
In
1,4-dioxane; 1,2-dimethoxyethane; water;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane; water / 15 h / Inert atmosphere; Reflux
2.1: lithium tert-butoxide; XPhos / tris-(dibenzylideneacetone)dipalladium(0) / 1,4-dioxane / 20 °C / Inert atmosphere
2.2: 12 h / 110 °C
With
sodium carbonate; lithium tert-butoxide; XPhos;
tris-(dibenzylideneacetone)dipalladium(0); tetrakis(triphenylphosphine) palladium(0);
In
1,4-dioxane; 1,2-dimethoxyethane; water;
