toluene-4-sulfonic acid 2-toluene 4-sulfonylmethoxyethyl ester

Base Information

Chemical Name:toluene-4-sulfonic acid 2-toluene 4-sulfonylmethoxyethyl ester
CAS No.:1608491-43-5
Molecular Formula:C₁₇H₂₀O₆S₂
Molecular Weight:384.474
Hs Code.:

Synonyms:toluene-4-sulfonic acid 2-toluene 4-sulfonylmethoxyethyl ester

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Chemical Property of toluene-4-sulfonic acid 2-toluene 4-sulfonylmethoxyethyl ester

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Technology Process of toluene-4-sulfonic acid 2-toluene 4-sulfonylmethoxyethyl ester

There total 5 articles about toluene-4-sulfonic acid 2-toluene 4-sulfonylmethoxyethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 2-{[(4-methylphenyl)sulfanyl]methoxy}ethyl-4-methylbenzene-1-sulfonate

: 1608491-43-5
toluene-4-sulfonic acid 2-toluene 4-sulfonylmethoxyethyl ester

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃; for 4h;
DOI:10.1039/c3cc46450d

Reference yield:

: 1608491-39-9
2-{[(4-methylphenyl)sulfanyl]methoxy}ethan-1-ol

: 1608491-43-5
toluene-4-sulfonic acid 2-toluene 4-sulfonylmethoxyethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine; trimethylamine hydrochloride / toluene / 0.17 h / 0 °C

1.2: 2.5 h / 0 - 20 °C

2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 4 h / 0 °C

With trimethylamine hydrochloride; triethylamine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; toluene;
DOI:10.1039/c3cc46450d

Reference yield:

: 623-13-2
4-methylphenyl methylsulfide

: 1608491-43-5
toluene-4-sulfonic acid 2-toluene 4-sulfonylmethoxyethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: N-chloro-succinimide / tetrachloromethane / 14.5 h / 20 °C

2.1: sodium hydride / mineral oil / 1.25 h / 0 °C

2.2: 5 h / 0 - 20 °C

3.1: triethylamine; trimethylamine hydrochloride / toluene / 0.17 h / 0 °C

3.2: 2.5 h / 0 - 20 °C

4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 4 h / 0 °C

With N-chloro-succinimide; trimethylamine hydrochloride; sodium hydride; triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrachloromethane; dichloromethane; toluene; mineral oil;
DOI:10.1039/c3cc46450d