2-[6-(2-Azido-phenyl)-4,5-dihydro-thiazolo[5,4-h]quinolin-4-yl]-ethylamine

Base Information

Chemical Name:2-[6-(2-Azido-phenyl)-4,5-dihydro-thiazolo[5,4-h]quinolin-4-yl]-ethylamine
CAS No.:145290-54-6
Molecular Formula:C₁₈H₁₆N₆S
Molecular Weight:348.431
Hs Code.:

Synonyms:2-[6-(2-Azido-phenyl)-4,5-dihydro-thiazolo[5,4-h]quinolin-4-yl]-ethylamine

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Chemical Property of 2-[6-(2-Azido-phenyl)-4,5-dihydro-thiazolo[5,4-h]quinolin-4-yl]-ethylamine

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Technology Process of 2-[6-(2-Azido-phenyl)-4,5-dihydro-thiazolo[5,4-h]quinolin-4-yl]-ethylamine

There total 5 articles about 2-[6-(2-Azido-phenyl)-4,5-dihydro-thiazolo[5,4-h]quinolin-4-yl]-ethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 145290-53-5
2-{2-[6-(2-Azido-phenyl)-4,5-dihydro-thiazolo[5,4-h]quinolin-4-yl]-ethyl}-isoindole-1,3-dione

: 145290-54-6
2-[6-(2-Azido-phenyl)-4,5-dihydro-thiazolo[5,4-h]quinolin-4-yl]-ethylamine

Guidance literature:: With hydrazine hydrate; In methanol; for 0.5h; Ambient temperature;
DOI:10.1021/ja00051a062

Reference yield:

: 145290-50-2
Acetic acid 2-[6-(2-azido-phenyl)-4,5-dihydro-thiazolo[5,4-h]quinolin-4-yl]-ethyl ester

: 145290-54-6
2-[6-(2-Azido-phenyl)-4,5-dihydro-thiazolo[5,4-h]quinolin-4-yl]-ethylamine

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / K₂CO₃, methanol / 0.25 h / Ambient temperature

2: 99 percent / Et₃N / CH₂Cl₂ / 0.17 h / 0 °C

3: 84 percent / dimethylformamide / 8 h / 50 °C

4: 94 percent / hydrazine hydrate / methanol; tetrahydrofuran / 0.5 h / Ambient temperature

With methanol; potassium carbonate; hydrazine hydrate; triethylamine; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja00155a010

Reference yield:

: 145290-52-4
Methanesulfonic acid 2-[6-(2-azido-phenyl)-4,5-dihydro-thiazolo[5,4-h]quinolin-4-yl]-ethyl ester

: 145290-54-6
2-[6-(2-Azido-phenyl)-4,5-dihydro-thiazolo[5,4-h]quinolin-4-yl]-ethylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / dimethylformamide / 8 h / 50 °C

2: 94 percent / hydrazine hydrate / methanol; tetrahydrofuran / 0.5 h / Ambient temperature

With hydrazine hydrate; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1021/ja00155a010