Technology Process of C22H36O8
There total 3 articles about C22H36O8 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
methyl-triphenylphosphonium iodide;
With
potassium tert-butylate;
In
tetrahydrofuran;
at 20 ℃;
for 0.25h;
3,5-bis-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-benzaldehyde;
In
tetrahydrofuran;
at 20 ℃;
for 2h;
Further stages.;
DOI:10.1021/ma0506233
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: n-BuLi / diethyl ether; hexane / 0.5 h / -78 °C
1.2: 60 percent / diethyl ether; hexane / 1 h / -78 °C
2.1: 59.2 percent / Ph3P; diethyl azodicarboxylate / tetrahydrofuran / 24 h / 20 °C
3.1: t-BuOK / tetrahydrofuran / 0.25 h / 20 °C
3.2: 83 percent / tetrahydrofuran / 2 h / 20 °C
With
n-butyllithium; potassium tert-butylate; triphenylphosphine; diethylazodicarboxylate;
In
tetrahydrofuran; diethyl ether; hexane;
2.1: Mitsunobu reaction / 3.2: Wittig reaction;
DOI:10.1021/ma0506233
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: 59.2 percent / Ph3P; diethyl azodicarboxylate / tetrahydrofuran / 24 h / 20 °C
2.1: t-BuOK / tetrahydrofuran / 0.25 h / 20 °C
2.2: 83 percent / tetrahydrofuran / 2 h / 20 °C
With
potassium tert-butylate; triphenylphosphine; diethylazodicarboxylate;
In
tetrahydrofuran;
1.1: Mitsunobu reaction / 2.2: Wittig reaction;
DOI:10.1021/ma0506233
