5-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-2-(phenylseleno)pentyl methyl carbonate

Base Information

Chemical Name:5-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-2-(phenylseleno)pentyl methyl carbonate
CAS No.:335164-83-5
Molecular Formula:C₂₉H₃₆O₄SeSi
Molecular Weight:555.648
Hs Code.:

Synonyms:5-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-2-(phenylseleno)pentyl methyl carbonate

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Chemical Property of 5-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-2-(phenylseleno)pentyl methyl carbonate

Chemical Property:

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Technology Process of 5-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-2-(phenylseleno)pentyl methyl carbonate

There total 4 articles about 5-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-2-(phenylseleno)pentyl methyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 79-22-1
methyl chloroformate

: 335164-82-4
5-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-2-(phenylseleno)-1-pentanol

: 335164-83-5
5-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-2-(phenylseleno)pentyl methyl carbonate

Guidance literature:: With pyridine; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1021/jo001124x

Reference yield:

: 5707-04-0
Phenylselenyl chloride

: 335164-83-5
5-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-2-(phenylseleno)pentyl methyl carbonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: Et₂NH / hexane / 0.5 h / 0 °C

1.2: hexane; CH₂Cl₂ / 0.5 h / -78 °C

2.1: 1.890 g / NaBH₄ / methanol / 1 h / 0 °C

3.1: 84 percent / pyridine / CH₂Cl₂ / 1 h / 0 °C

With pyridine; sodium tetrahydroborate; diethylamine; In methanol; hexane; dichloromethane;
DOI:10.1021/jo001124x

Reference yield:

: 131216-47-2
5-(tert-butyldiphenylsilyloxy)pentanal

: 335164-83-5
5-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-2-(phenylseleno)pentyl methyl carbonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: Et₂NH / hexane / 0.5 h / 0 °C

1.2: hexane; CH₂Cl₂ / 0.5 h / -78 °C

2.1: 1.890 g / NaBH₄ / methanol / 1 h / 0 °C

3.1: 84 percent / pyridine / CH₂Cl₂ / 1 h / 0 °C

With pyridine; sodium tetrahydroborate; diethylamine; In methanol; hexane; dichloromethane;
DOI:10.1021/jo001124x