β-(6-benzophenanthryl)-2,3-dimethoxystyrene

Base Information

Chemical Name:β-(6-benzophenanthryl)-2,3-dimethoxystyrene
CAS No.:160086-29-3
Molecular Formula:C₂₈H₂₂O₂
Molecular Weight:390.481
Hs Code.:

β-(6-benzo<c>phenanthryl)-2,3-dimethoxystyrene

Synonyms:β-(6-benzophenanthryl)-2,3-dimethoxystyrene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of β-(6-benzophenanthryl)-2,3-dimethoxystyrene

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Technology Process of β-(6-benzophenanthryl)-2,3-dimethoxystyrene

There total 3 articles about β-(6-benzophenanthryl)-2,3-dimethoxystyrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 6-(benzophenanthryl)methyltriphenylphosphonium bromide

: 86-51-1
2,3-dimethyoxybenzaldehyde

: 160086-29-3
β-(6-benzophenanthryl)-2,3-dimethoxystyrene

Guidance literature:: With sodium hydroxide; 18-crown-6 ether; In dichloromethane; water;
DOI:10.1021/jo9806613

Reference yield:

: 2381-34-2
6-methylbenzo[c]phenanthrene

: 160086-29-3
β-(6-benzophenanthryl)-2,3-dimethoxystyrene

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / NBS, benzoyl peroxide / CCl₄ / 2 h / Heating

2: 90 percent / toluene / Heating

3: 94 percent / 18-crown-6, NaOH / CH₂Cl₂; H₂O

With sodium hydroxide; N-Bromosuccinimide; Perbenzoic acid; 18-crown-6 ether; In tetrachloromethane; dichloromethane; water; toluene;
DOI:10.1021/jo9806613

Reference yield:

: 213742-71-3
6-bromomethylbenzophenanthrene

: 160086-29-3
β-(6-benzophenanthryl)-2,3-dimethoxystyrene

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / toluene / Heating

2: 94 percent / 18-crown-6, NaOH / CH₂Cl₂; H₂O

With sodium hydroxide; 18-crown-6 ether; In dichloromethane; water; toluene;
DOI:10.1021/jo9806613