1-((6-chloropyridin-3-yl)methyl)-5-(2,4-dimethylphenyl)-1,3,5-hexahydrotriazine-2-(N-nitro)imine

Base Information

Chemical Name:1-((6-chloropyridin-3-yl)methyl)-5-(2,4-dimethylphenyl)-1,3,5-hexahydrotriazine-2-(N-nitro)imine
CAS No.:1200835-67-1
Molecular Formula:C₁₇H₁₉ClN₆O₂
Molecular Weight:374.83
Hs Code.:

Synonyms:1-((6-chloropyridin-3-yl)methyl)-5-(2,4-dimethylphenyl)-1,3,5-hexahydrotriazine-2-(N-nitro)imine

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Chemical Property of 1-((6-chloropyridin-3-yl)methyl)-5-(2,4-dimethylphenyl)-1,3,5-hexahydrotriazine-2-(N-nitro)imine

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Technology Process of 1-((6-chloropyridin-3-yl)methyl)-5-(2,4-dimethylphenyl)-1,3,5-hexahydrotriazine-2-(N-nitro)imine

There total 4 articles about 1-((6-chloropyridin-3-yl)methyl)-5-(2,4-dimethylphenyl)-1,3,5-hexahydrotriazine-2-(N-nitro)imine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 70258-18-3
2-chloro-5-(chloromethyl)pyridine

: 1200835-88-6
C₁₁H₁₅N₅O₂

: 1200835-67-1
1-((6-chloropyridin-3-yl)methyl)-5-(2,4-dimethylphenyl)-1,3,5-hexahydrotriazine-2-(N-nitro)imine

Guidance literature:: With cesium chloride; potassium carbonate; In N,N-dimethyl-formamide; acetonitrile; at 55 ℃; for 66h;
DOI:10.1002/jhet.642

Reference yield:

: 1325765-38-5
C₉H₁₁N*ClH

: 1200835-67-1
1-((6-chloropyridin-3-yl)methyl)-5-(2,4-dimethylphenyl)-1,3,5-hexahydrotriazine-2-(N-nitro)imine

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / ethanol / Reflux

2: cesium chloride; potassium carbonate / N,N-dimethyl-formamide; acetonitrile / 66 h / 55 °C

With hydrogenchloride; cesium chloride; potassium carbonate; In ethanol; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/jhet.642

Reference yield:

: 95-68-1
2,4-Xylidine

: 1200835-67-1
1-((6-chloropyridin-3-yl)methyl)-5-(2,4-dimethylphenyl)-1,3,5-hexahydrotriazine-2-(N-nitro)imine

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogenchloride / diethyl ether; water

2: ethanol / 1 h / 25 °C

3: hydrogenchloride / ethanol / Reflux

4: cesium chloride; potassium carbonate / N,N-dimethyl-formamide; acetonitrile / 66 h / 55 °C

With hydrogenchloride; cesium chloride; potassium carbonate; In diethyl ether; ethanol; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/jhet.642