C₁₃H₁₂F₃IO₃S

Base Information

Chemical Name:C₁₃H₁₂F₃IO₃S
CAS No.:1419389-49-3
Molecular Formula:C₁₃H₁₂F₃IO₃S
Molecular Weight:432.202
Hs Code.:

C<sub>13</sub>H<sub>12</sub>F<sub>3</sub>IO<sub>3</sub>S

Synonyms:C₁₃H₁₂F₃IO₃S

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Chemical Property of C₁₃H₁₂F₃IO₃S

Chemical Property:

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Technology Process of C₁₃H₁₂F₃IO₃S

There total 1 articles about C₁₃H₁₂F₃IO₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 52289-93-7
o-Methoxybenzyl bromide

: 1419389-49-3
C₁₃H₁₂F₃IO₃S

Guidance literature:: Multi-step reaction with 6 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -25 °C

1.2: 2 h / 0 °C

2.1: lithium hydroxide / tetrahydrofuran; methanol; water / 50 °C

2.2: 4 h / 0 °C

3.1: triethylsilane; trifluoroacetic acid / 40 °C / Cooling with ice

4.1: N-iodo-succinimide; trifluoroacetic acid / acetonitrile / 20 °C / Cooling with ice

5.1: boron tribromide / dichloromethane / 6 h / -78 - 20 °C

6.1: pyridine / dichloromethane / 3.33 h / 20 °C / Inert atmosphere; Cooling with ice

With pyridine; triethylsilane; N-iodo-succinimide; boron tribromide; trifluoroacetic acid; lithium hydroxide; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; dichloromethane; water; acetonitrile;

Reference yield: 78.0%

: 1228553-33-0
[(S)-2-methyl-1-((S)-2-{5-[4-(4,4,5,5 tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-1H-imidazol-2-yl}-pyrrolidine-1-carbonyl)-propyl]-carbamic acid methyl ester

: 1419389-49-3
C₁₃H₁₂F₃IO₃S

: 1419389-51-7
C₃₃H₃₇F₃N₄O₆S

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In 1,2-dimethoxyethane; water; at 90 ℃; Inert atmosphere;

Reference yield:

: 1228553-33-0
[(S)-2-methyl-1-((S)-2-{5-[4-(4,4,5,5 tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-1H-imidazol-2-yl}-pyrrolidine-1-carbonyl)-propyl]-carbamic acid methyl ester

: 1419389-49-3
C₁₃H₁₂F₃IO₃S

: 1419385-31-1
C₅₀H₆₀N₈O₆

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,2-dimethoxyethane; water / 90 °C / Inert atmosphere

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,2-dimethoxyethane; water / 90 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In 1,2-dimethoxyethane; water;