N-methyl-N-<3-(2,6,6-trimethyl-1-cyclohexenyl)-2-propinyl>-1-naphthalinmethanamin

Base Information

Chemical Name:N-methyl-N-<3-(2,6,6-trimethyl-1-cyclohexenyl)-2-propinyl>-1-naphthalinmethanamin
CAS No.:104257-78-5
Molecular Formula:C₂₄H₂₉N
Molecular Weight:331.501
Hs Code.:

Synonyms:N-methyl-N-<3-(2,6,6-trimethyl-1-cyclohexenyl)-2-propinyl>-1-naphthalinmethanamin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-methyl-N-<3-(2,6,6-trimethyl-1-cyclohexenyl)-2-propinyl>-1-naphthalinmethanamin

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Technology Process of N-methyl-N-<3-(2,6,6-trimethyl-1-cyclohexenyl)-2-propinyl>-1-naphthalinmethanamin

There total 3 articles about N-methyl-N-<3-(2,6,6-trimethyl-1-cyclohexenyl)-2-propinyl>-1-naphthalinmethanamin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1892-05-3
2-ethynyl-1,3,3-trimethyl-1-cyclohexene

: 14489-75-9
N-methyl-1-naphthalenemethylamine

: 104257-78-5
N-methyl-N-<3-(2,6,6-trimethyl-1-cyclohexenyl)-2-propinyl>-1-naphthalinmethanamin

Guidance literature:: zinc(II) chloride; In 1,4-dioxane; at 100 ℃; for 2h;
DOI:10.1016/S0040-4020(01)91373-0

Reference yield: 30.0%

: 2,2,6-Trimethyl-1-[3-(methyl-naphthalen-1-ylmethyl-amino)-prop-1-ynyl]-cyclohexanol

: 104257-78-5
N-methyl-N-<3-(2,6,6-trimethyl-1-cyclohexenyl)-2-propinyl>-1-naphthalinmethanamin

Guidance literature:: With trichlorophosphate; In pyridine; at 100 ℃; for 1h;
DOI:10.1016/S0040-4020(01)91373-0

Reference yield:

: 2408-37-9
2,2,6-trimethylcyclohexan-1-one

: 104257-78-5
N-methyl-N-<3-(2,6,6-trimethyl-1-cyclohexenyl)-2-propinyl>-1-naphthalinmethanamin

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / tetrahydrofuran / 16 h / Ambient temperature

2: 30 percent / POCl₃ / pyridine / 1 h / 100 °C

With trichlorophosphate; In tetrahydrofuran; pyridine;
DOI:10.1016/S0040-4020(01)91373-0