N-(3,4-Dimethyl-5-isoxazolyl)-N-[(2-methoxyethoxy)methyl]-2'-[(3-methyl-2-oxo-1-imidazolidinyl)methyl]-4'-(2-oxazolyl)[1,1'-biphenyl]-2-sulfonamide

Base Information

Chemical Name:N-(3,4-Dimethyl-5-isoxazolyl)-N-[(2-methoxyethoxy)methyl]-2'-[(3-methyl-2-oxo-1-imidazolidinyl)methyl]-4'-(2-oxazolyl)[1,1'-biphenyl]-2-sulfonamide
CAS No.:195447-69-9
Molecular Formula:C₂₉H₃₃N₅O₇S
Molecular Weight:595.676
Hs Code.:

Synonyms:N-(3,4-Dimethyl-5-isoxazolyl)-N-[(2-methoxyethoxy)methyl]-2'-[(3-methyl-2-oxo-1-imidazolidinyl)methyl]-4'-(2-oxazolyl)[1,1'-biphenyl]-2-sulfonamide

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Chemical Property of N-(3,4-Dimethyl-5-isoxazolyl)-N-[(2-methoxyethoxy)methyl]-2'-[(3-methyl-2-oxo-1-imidazolidinyl)methyl]-4'-(2-oxazolyl)[1,1'-biphenyl]-2-sulfonamide

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Technology Process of N-(3,4-Dimethyl-5-isoxazolyl)-N-[(2-methoxyethoxy)methyl]-2'-[(3-methyl-2-oxo-1-imidazolidinyl)methyl]-4'-(2-oxazolyl)[1,1'-biphenyl]-2-sulfonamide

There total 5 articles about N-(3,4-Dimethyl-5-isoxazolyl)-N-[(2-methoxyethoxy)methyl]-2'-[(3-methyl-2-oxo-1-imidazolidinyl)methyl]-4'-(2-oxazolyl)[1,1'-biphenyl]-2-sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 176961-44-7
N-(3,4-Dimethyl-5-isoxazolyl)-2'-formyl-N-[(2-methoxyethoxy)methyl]-4'-(2-oxazolyl)-[1,1'-biphenyl]-2-sulfonamide

: 195447-69-9
N-(3,4-Dimethyl-5-isoxazolyl)-N-[(2-methoxyethoxy)methyl]-2'-[(3-methyl-2-oxo-1-imidazolidinyl)methyl]-4'-(2-oxazolyl)[1,1'-biphenyl]-2-sulfonamide

Guidance literature:: Multi-step reaction with 5 steps

1: NaBH₄ / methanol / 2.5 h / 0 °C

2: 165 mg / CBr₄; PPh₃ / dimethylformamide / 2.5 h / 0 °C

3: 3A molecular sieves; AcOH / CH₂Cl₂ / 0.17 h

4: Na(AcO)3BH / CH₂Cl₂ / 12 h / 20 °C

5: CH₂Cl₂ / 24 h / 20 °C

With sodium tetrahydroborate; carbon tetrabromide; 3 A molecular sieve; sodium tris(acetoxy)borohydride; acetic acid; triphenylphosphine; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm020289q

Reference yield:

: 195447-19-9
2'-hydroxymethyl-4'-oxazol-2-yl-biphenyl-2-sulfonic acid (3,4-dimethyl-isoxazol-5-yl)-(2-methoxy-ethoxymethyl)-amide

: 195447-69-9
N-(3,4-Dimethyl-5-isoxazolyl)-N-[(2-methoxyethoxy)methyl]-2'-[(3-methyl-2-oxo-1-imidazolidinyl)methyl]-4'-(2-oxazolyl)[1,1'-biphenyl]-2-sulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: 165 mg / CBr₄; PPh₃ / dimethylformamide / 2.5 h / 0 °C

2: 3A molecular sieves; AcOH / CH₂Cl₂ / 0.17 h

3: Na(AcO)3BH / CH₂Cl₂ / 12 h / 20 °C

4: CH₂Cl₂ / 24 h / 20 °C

With carbon tetrabromide; 3 A molecular sieve; sodium tris(acetoxy)borohydride; acetic acid; triphenylphosphine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm020289q

Reference yield:

: 195447-20-2
2'-(bromomethyl)-N-(3,4-dimethyl-5-isoxazolyl)-N-[(2-methoxyethoxy)methyl]-4'-(2-oxazolyl)[1,1'-biphenyl]-2-sulfonamide

: 195447-69-9
N-(3,4-Dimethyl-5-isoxazolyl)-N-[(2-methoxyethoxy)methyl]-2'-[(3-methyl-2-oxo-1-imidazolidinyl)methyl]-4'-(2-oxazolyl)[1,1'-biphenyl]-2-sulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: 3A molecular sieves; AcOH / CH₂Cl₂ / 0.17 h

2: Na(AcO)3BH / CH₂Cl₂ / 12 h / 20 °C

3: CH₂Cl₂ / 24 h / 20 °C

With 3 A molecular sieve; sodium tris(acetoxy)borohydride; acetic acid; In dichloromethane;
DOI:10.1021/jm020289q