(2S,3S,4R)-1-O-(α-D-galactopyranosyl)-4-O-(hexacosanoyl)-2-(((N-(6-azidohexanoyl)-Val-Cit-4-aminobenzyloxy)carbonyl)amino)nonane-1,3,4-triol

Base Information

Chemical Name:(2S,3S,4R)-1-O-(α-D-galactopyranosyl)-4-O-(hexacosanoyl)-2-(((N-(6-azidohexanoyl)-Val-Cit-4-aminobenzyloxy)carbonyl)amino)nonane-1,3,4-triol
CAS No.:1613321-20-2
Molecular Formula:C₆₆H₁₁₇N₉O₁₅
Molecular Weight:1276.71
Hs Code.:

Synonyms:(2S,3S,4R)-1-O-(α-D-galactopyranosyl)-4-O-(hexacosanoyl)-2-(((N-(6-azidohexanoyl)-Val-Cit-4-aminobenzyloxy)carbonyl)amino)nonane-1,3,4-triol

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Chemical Property of (2S,3S,4R)-1-O-(α-D-galactopyranosyl)-4-O-(hexacosanoyl)-2-(((N-(6-azidohexanoyl)-Val-Cit-4-aminobenzyloxy)carbonyl)amino)nonane-1,3,4-triol

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Technology Process of (2S,3S,4R)-1-O-(α-D-galactopyranosyl)-4-O-(hexacosanoyl)-2-(((N-(6-azidohexanoyl)-Val-Cit-4-aminobenzyloxy)carbonyl)amino)nonane-1,3,4-triol

There total 5 articles about (2S,3S,4R)-1-O-(α-D-galactopyranosyl)-4-O-(hexacosanoyl)-2-(((N-(6-azidohexanoyl)-Val-Cit-4-aminobenzyloxy)carbonyl)amino)nonane-1,3,4-triol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1613321-19-9
(2S,3S,4R)-2-amino-1-O-(α-D-galactopyranosyl)-4-O-(hexacosanoyl)nonane-1,3,4-triol

: 1613321-02-0
N-(6-azidohexanoyl)-Val-Cit-4-aminobenzyl 4-nitrophenyl carbonate

: 1613321-20-2
(2S,3S,4R)-1-O-(α-D-galactopyranosyl)-4-O-(hexacosanoyl)-2-(((N-(6-azidohexanoyl)-Val-Cit-4-aminobenzyloxy)carbonyl)amino)nonane-1,3,4-triol

Guidance literature:: With triethylamine; In pyridine; at 20 ℃; for 32h; Inert atmosphere;

Reference yield:

: 79598-53-1
6-azidohexanoic acid

: 1613321-20-2
(2S,3S,4R)-1-O-(α-D-galactopyranosyl)-4-O-(hexacosanoyl)-2-(((N-(6-azidohexanoyl)-Val-Cit-4-aminobenzyloxy)carbonyl)amino)nonane-1,3,4-triol

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / dichloromethane / 0.5 h / 0 °C

2: methanol; dichloromethane / 2.58 h / 0 - 20 °C

3: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 41 h / 20 °C / Inert atmosphere

4: triethylamine / pyridine / 32 h / 20 °C / Inert atmosphere

With triethylamine; N-ethyl-N,N-diisopropylamine; In pyridine; methanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1613321-01-9
N-(6-azidohexanoyl)-Val-Cit-4-aminobenzyl alcohol

: 1613321-20-2
(2S,3S,4R)-1-O-(α-D-galactopyranosyl)-4-O-(hexacosanoyl)-2-(((N-(6-azidohexanoyl)-Val-Cit-4-aminobenzyloxy)carbonyl)amino)nonane-1,3,4-triol

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 41 h / 20 °C / Inert atmosphere

2: triethylamine / pyridine / 32 h / 20 °C / Inert atmosphere

With triethylamine; N-ethyl-N,N-diisopropylamine; In pyridine; N,N-dimethyl-formamide;