tert-butyl (1-(4-(3-(dimethylamino)-2-phenylacryloyl)phenyl)cyclobutyl)carbamate

Base Information

• Chemical Name: tert-butyl (1-(4-(3-(dimethylamino)-2-phenylacryloyl)phenyl)cyclobutyl)carbamate
• CAS No.: 1247897-74-0
• Molecular Formula: C₂₆H₃₂N₂O₃
• Molecular Weight: 420.552

Synonyms:tert-butyl (1-(4-(3-(dimethylamino)-2-phenylacryloyl)phenyl)cyclobutyl)carbamate

Chemical Property of tert-butyl (1-(4-(3-(dimethylamino)-2-phenylacryloyl)phenyl)cyclobutyl)carbamate

Chemical Property:

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Technology Process of tert-butyl (1-(4-(3-(dimethylamino)-2-phenylacryloyl)phenyl)cyclobutyl)carbamate

There total 1 articles about tert-butyl (1-(4-(3-(dimethylamino)-2-phenylacryloyl)phenyl)cyclobutyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

tert-butyl 1-(4-(2-phenylacetyl)phenyl)cyclobutylcarbamate (1032349-98-6) + N,N-dimethyl-formamide dimethyl acetal (4637-24-5) → tert-butyl (1-(4-(3-(dimethylamino)-2-phenylacryloyl)phenyl)cyclobutyl)carbamate (1247897-74-0)

Guidance literature:

at 80 ℃; for 18h; Inert atmosphere;

Reference yield: 41.0%

tert-butyl (1-(4-(3-(dimethylamino)-2-phenylacryloyl)phenyl)cyclobutyl)carbamate (1247897-74-0) + 1-amino-5,5-dimethylcyclohexen-3-one (873-95-0) → tert-butyl (1-(4-(7,7-dimethyl-5-oxo-3-phenyl-5,6,7,8-tetrahydroquinolin-2-yl)phenyl)cyclobutyl)carbamate (1313440-09-3)

Guidance literature:

With acetic acid; at 100 ℃; for 2h; Inert atmosphere; Molecular sieve;

Reference yield: 37.0%

tert-butyl (1-(4-(3-(dimethylamino)-2-phenylacryloyl)phenyl)cyclobutyl)carbamate (1247897-74-0) + 3-amino-cyclohex-2-enone (5220-49-5) → tert-butyl (1-(4-(5-oxo-3-phenyl-5,6,7,8-tetrahydroquinolin-2-yl)phenyl)cyclobutyl)carbamate (1313439-86-9)

Guidance literature:

With acetic acid; at 100 ℃; for 2h; Inert atmosphere; Molecular sieve;

upstream raw materials:

tert-butyl 1-(4-(2-phenylacetyl)phenyl)cyclobutylcarbamate

N,N-dimethyl-formamide dimethyl acetal

Downstream raw materials:

tert-butyl (1-(4-(5-oxo-3-phenyl-5,6,7,8-tetrahydro-1,6-naphthyridin-2-yl)phenyl)cyclobutyl)carbamate

tert-butyl (1-(4-(5-oxo-3-phenyl-5,6,7,8-tetrahydroquinolin-2-yl)phenyl)cyclobutyl)carbamate

tert-butyl (1-(4-(7,7-dimethyl-5-oxo-3-phenyl-5,6,7,8-tetrahydroquinolin-2-yl)phenyl)cyclobutyl)carbamate

tert-butyl (1-(4-(5-oxo-3-phenyl-6,7,8,9-tetrahydro-5H-cyclohepta[b]pyridin-2-yl)phenyl)cyclobutyl)carbamate

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