1,11-bis[3-(2,2,2-trifluoro-1-p-tolyl-ethoxysulfonyl)propyl]-3,4,8,9,10,11-hexahydro-2H-13-oxa-6,11-diaza-1-azoniapentacene tetrafluoroborate

Base Information

Chemical Name:1,11-bis[3-(2,2,2-trifluoro-1-p-tolyl-ethoxysulfonyl)propyl]-3,4,8,9,10,11-hexahydro-2H-13-oxa-6,11-diaza-1-azoniapentacene tetrafluoroborate
CAS No.:1415743-35-9
Molecular Formula:BF₄*C₄₂H₄₄F₆N₃O₇S₂
Molecular Weight:967.754
Hs Code.:

Synonyms:1,11-bis[3-(2,2,2-trifluoro-1-p-tolyl-ethoxysulfonyl)propyl]-3,4,8,9,10,11-hexahydro-2H-13-oxa-6,11-diaza-1-azoniapentacene tetrafluoroborate

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Chemical Property of 1,11-bis[3-(2,2,2-trifluoro-1-p-tolyl-ethoxysulfonyl)propyl]-3,4,8,9,10,11-hexahydro-2H-13-oxa-6,11-diaza-1-azoniapentacene tetrafluoroborate

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Technology Process of 1,11-bis[3-(2,2,2-trifluoro-1-p-tolyl-ethoxysulfonyl)propyl]-3,4,8,9,10,11-hexahydro-2H-13-oxa-6,11-diaza-1-azoniapentacene tetrafluoroborate

There total 6 articles about 1,11-bis[3-(2,2,2-trifluoro-1-p-tolyl-ethoxysulfonyl)propyl]-3,4,8,9,10,11-hexahydro-2H-13-oxa-6,11-diaza-1-azoniapentacene tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 1415743-30-4
3-[7-(tert-butyldimethylsilanyloxy)-3,4-dihydro-2H-quinolin-1-yl]propane-1-sulfonic acid 2,2,2-trifluoro-1-p-tolyl-ethyl ester

: 1415743-35-9
1,11-bis[3-(2,2,2-trifluoro-1-p-tolyl-ethoxysulfonyl)propyl]-3,4,8,9,10,11-hexahydro-2H-13-oxa-6,11-diaza-1-azoniapentacene tetrafluoroborate

Guidance literature:: With hydrogenchloride; In ethanol; water; at 80 ℃; for 2h;
DOI:10.1021/jo302065u

Reference yield:

: 1415743-28-0
3-chloropropane-1-sulfonic acid 2,2,2-trifluoro-1-p-tolyl-ethyl ester

: 1415743-35-9
1,11-bis[3-(2,2,2-trifluoro-1-p-tolyl-ethoxysulfonyl)propyl]-3,4,8,9,10,11-hexahydro-2H-13-oxa-6,11-diaza-1-azoniapentacene tetrafluoroborate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium iodide / acetone / 16 h / Reflux

2: potassium carbonate / N,N-dimethyl-formamide / 24 h / 70 °C

3: hydrogenchloride / water; ethanol / 2 h / 80 °C

With hydrogenchloride; potassium carbonate; sodium iodide; In ethanol; water; N,N-dimethyl-formamide; acetone;
DOI:10.1021/jo302065u

Reference yield:

: 1415743-29-1
3-iodopropane-1-sulfonic acid 2,2,2-trifluoro-1-p-tolyl-ethyl ester

: 1415743-35-9
1,11-bis[3-(2,2,2-trifluoro-1-p-tolyl-ethoxysulfonyl)propyl]-3,4,8,9,10,11-hexahydro-2H-13-oxa-6,11-diaza-1-azoniapentacene tetrafluoroborate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 24 h / 70 °C

2: hydrogenchloride / water; ethanol / 2 h / 80 °C

With hydrogenchloride; potassium carbonate; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jo302065u