oxiran-2-ylmethyl 2-amino-6-(3,5-dimethoxyphenyl)-4-(2-(oxiran-2-ylmethoxy)-2-oxoethyl)-4H-chromene-3-carboxylate

Base Information

Chemical Name:oxiran-2-ylmethyl 2-amino-6-(3,5-dimethoxyphenyl)-4-(2-(oxiran-2-ylmethoxy)-2-oxoethyl)-4H-chromene-3-carboxylate
CAS No.:1379536-06-7
Molecular Formula:C₂₆H₂₇NO₉
Molecular Weight:497.502
Hs Code.:

Synonyms:oxiran-2-ylmethyl 2-amino-6-(3,5-dimethoxyphenyl)-4-(2-(oxiran-2-ylmethoxy)-2-oxoethyl)-4H-chromene-3-carboxylate

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Chemical Property of oxiran-2-ylmethyl 2-amino-6-(3,5-dimethoxyphenyl)-4-(2-(oxiran-2-ylmethoxy)-2-oxoethyl)-4H-chromene-3-carboxylate

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Technology Process of oxiran-2-ylmethyl 2-amino-6-(3,5-dimethoxyphenyl)-4-(2-(oxiran-2-ylmethoxy)-2-oxoethyl)-4H-chromene-3-carboxylate

There total 6 articles about oxiran-2-ylmethyl 2-amino-6-(3,5-dimethoxyphenyl)-4-(2-(oxiran-2-ylmethoxy)-2-oxoethyl)-4H-chromene-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 1318165-60-4
allyl 4-(2-(allyloxy)-2-oxoethyl)-2-amino-6-(3,5-dimethoxyphenyl)-4H-chromene-3-carboxylate

: 1379536-06-7
oxiran-2-ylmethyl 2-amino-6-(3,5-dimethoxyphenyl)-4-(2-(oxiran-2-ylmethoxy)-2-oxoethyl)-4H-chromene-3-carboxylate

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 - 20 ℃; for 25h; Inert atmosphere;
DOI:10.1021/jm300515q

Reference yield:

: 1761-61-1
5-bromosalicyclaldehyde

: 1379536-06-7
oxiran-2-ylmethyl 2-amino-6-(3,5-dimethoxyphenyl)-4-(2-(oxiran-2-ylmethoxy)-2-oxoethyl)-4H-chromene-3-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1.1: palladium diacetate; potassium carbonate; triphenylphosphine / 1,2-dimethoxyethane; water / 24 h / 20 °C

2.1: trichlorophosphate / dichloromethane / 4 h / 80 °C

2.2: 1 h / 60 °C

3.1: sodium / 2 h / 20 °C

4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 25 h / 0 - 20 °C / Inert atmosphere

With palladium diacetate; sodium; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; trichlorophosphate; In 1,2-dimethoxyethane; dichloromethane; water; 1.1: Suzuki coupling;
DOI:10.1021/jm300515q

Reference yield:

: 1063714-84-0
2-hydroxy-5-(3',5'-dimethoxyphenyl)benzaldehyde

: 1379536-06-7
oxiran-2-ylmethyl 2-amino-6-(3,5-dimethoxyphenyl)-4-(2-(oxiran-2-ylmethoxy)-2-oxoethyl)-4H-chromene-3-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: trichlorophosphate / dichloromethane / 4 h / 80 °C

1.2: 1 h / 60 °C

2.1: sodium / 2 h / 20 °C

3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 25 h / 0 - 20 °C / Inert atmosphere

With sodium; 3-chloro-benzenecarboperoxoic acid; trichlorophosphate; In dichloromethane;
DOI:10.1021/jm300515q